Real-Time Observation of Nanoscale Kink Band Mediated Plasticity in Ion-Irradiated Graphite: An In Situ TEM Study

  • 0Department of Mechanical Engineering, The Pennsylvania State University, University Park, PA 16802, USA.

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Summary

This summary is machine-generated.

Ion irradiation transforms brittle graphite into a ductile material by forming kink bands. These kink bands accommodate strain, preventing failure and enhancing toughness in nuclear reactor components.

Area Of Science

  • Materials Science
  • Nuclear Engineering
  • Solid Mechanics

Background

  • Graphite IG-110, a synthetic polycrystalline material, is utilized as a neutron moderator in nuclear reactors.
  • Graphite exhibits inherent brittleness, which is exacerbated by radiation damage at room temperature.

Purpose Of The Study

  • To investigate the effects of ion irradiation on pre-existing defects in graphite.
  • To understand how these defects influence the material's response to external loads.

Main Methods

  • Micropillar compression tests were conducted.
  • In situ nanoindentation within Transmission Electron Microscopy (TEM) was employed for both pristine and irradiated samples.

Main Results

  • Pristine graphite samples failed catastrophically under load.
  • Ion-irradiated graphite (2.8 MeV Au<sup>2+</sup>, 4.378 × 10<sup>14</sup> cm<sup>-2</sup>) exhibited extensive plasticity and no failure at room temperature.
  • In situ TEM revealed nanoscale kink band structures that accommodated large strains by closing defects and cracks.

Conclusions

  • Compressive stress from ion irradiation induces kink bands by transforming buckled basal layers.
  • Applied mechanical load promotes kink band nucleation and motion, enabling significant plastic strain accommodation.
  • Graphite's microstructural non-uniformity localizes strain, making kink bands the primary mechanism for enhanced toughness in this brittle material.