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Protocol for electrocatalytic hydrogenation of 5-hydroxymethylfurfural using H and flow cells
Wenbin Zhang1, Felix Ofori Boakye1, Guanwu Lian1
1Institute for Advanced Study, Shenzhen University, Shenzhen, Guangdong 518060, China.
None:
Recently, there has been a growing interest in using sustainable energy to decrease lignin monomers to generate high-value-added products. Here, we present a protocol for electrocatalytic hydrogenation of 5-hydroxymethylfurfural. We describe steps for catalyst preparation, performing electrocatalytic experiments, high-performance liquid chromatography analysis, and in situ infrared reflection-absorption spectroscopy testing. The synthesized catalyst used in this reaction exhibits enhanced selectivity and Faradaic efficiency in NaClO4 solution. For complete details on the use and execution of this protocol, please refer to Zhang et al.1.
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