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Solid-state Graft Copolymer Electrolytes for Lithium Battery Applications
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A-LLTO Nanoparticles Embedded Composite Solid Polymer Electrolyte for Room Temperature Operational Li-metal

Rohan Paste1,2, Yu-Te Chen1,2, Krishna Borde3

  • 1Department of Materials Science and Engineering, National Yang Ming Chiao Tung University, Hsinchu, 300, Taiwan (ROC).

Small (Weinheim an Der Bergstrasse, Germany)
|May 3, 2024
PubMed
Summary

This study introduces a new composite solid polymer electrolyte with aluminum-doped Li-La-Ti-oxide nanofillers for advanced solid-state batteries. The CAL-10% material shows high ionic conductivity and stable performance, paving the way for next-generation energy storage.

Keywords:
A‐LLTO nanoparticlesactive fillersjeffamine composite polymer electrolytesuperior ionic conductivity

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Area of Science:

  • Materials Science
  • Electrochemistry
  • Energy Storage

Background:

  • Lithium-ion batteries are crucial for electric vehicles but face limitations in energy demands.
  • Solid-state batteries (SSBs) offer a promising alternative for enhanced safety and energy density.
  • Development of robust and reliable solid electrolytes is key for advancing SSB technology.

Purpose of the Study:

  • To develop a novel self-healing composite solid polymer electrolyte (CSPE) for solid-state batteries.
  • To investigate the effect of aluminum-doped (Li0.33La0.56)1.005Ti0.99Al0.01O3 (A-LLTO) nanofillers on electrolyte properties.
  • To evaluate the electrochemical performance of the developed solid electrolyte in a CR-2032 cell.

Main Methods:

  • Synthesized a CSPE matrix using Jeffamine ED-2003 and Benzene-1,3,5-tricarbaldehyde crosslinker in DMF/LiPF6.
  • Incorporated varying amounts (5-12.5%) of A-LLTO nanofillers into the CSPE matrix.
  • Fabricated and tested CR-2032 coin cells with LiFePO4 (LFP) cathodes and Li anodes.

Main Results:

  • The composite electrolyte (CAL-10%) exhibited an ionic conductivity of 1.1 × 10-3 S cm-1 at room temperature.
  • Uniform dispersion of A-LLTO nanofillers formed a percolation network, enhancing Li+ ion diffusion.
  • The LFP║CAL-10%║Li cell demonstrated a high initial discharge capacity of ~165 mAh g-1 at 0.1C for 120 cycles with 98.85% coulombic efficiency.

Conclusions:

  • The novel CSPE with A-LLTO nanofillers shows excellent ionic conductivity and electrochemical stability.
  • The developed material is a promising candidate for high-performance solid-state batteries.
  • This advancement contributes to the development of safer and more reliable next-generation energy storage solutions.