Magnetic domain wall dynamics studied by in-situ Lorentz microscopy with aid of custom-made Hall-effect sensor holder

  • 0Tampere Microscopy Center, Tampere University, P.O. Box 692, 33014 Tampere University, Finland.

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Summary

This summary is machine-generated.

We developed a Hall-effect sensor holder for magnetic flux density measurements inside a transmission electron microscope (TEM). This tool enabled studying magnetic domain wall dynamics, revealing lamellar carbides as strong pinning sites.

Area Of Science

  • Materials Science
  • Condensed Matter Physics
  • Magnetism

Background

  • Understanding magnetic domain wall (DW) behavior is crucial for magnetic materials.
  • In-situ characterization within a transmission electron microscope (TEM) offers unique insights.
  • Quantifying magnetic fields generated by TEM components is essential for controlled experiments.

Purpose Of The Study

  • To develop and validate a custom Hall-effect sensor holder for in-situ magnetic field measurement inside a TEM.
  • To investigate the dynamics of magnetic domain walls in a ferritic-pearlitic steel under an externally applied magnetic field.
  • To correlate experimental observations of DW behavior with micromagnetic simulations.

Main Methods

  • Fabrication of a custom Hall-effect sensor holder for precise magnetic flux density measurements within a TEM.
  • In-situ Lorentz microscopy to observe magnetic domain wall (DW) dynamics.
  • Application of an external magnetic field using the TEM's objective lens.
  • Dynamical micromagnetic simulations to model DW behavior.

Main Results

  • The objective lens exhibits a nearly linear response, with near-zero field when switched off.
  • Magnetic domain walls in the ferritic matrix perpendicular to lamellar carbides initiate movement around 10 mT.
  • DWs within globular carbides disappear around 160 mT, with saturation near 210 mT.
  • Lamellar carbides act as strong pinning sites, retaining DWs up to 288 mT.
  • Micromagnetic simulations successfully reproduced the experimental observation of DW disappearance in globular carbides.

Conclusions

  • The custom Hall-effect sensor holder is effective for in-situ magnetic field quantification in a TEM.
  • Lamellar carbides in ferritic-pearlitic steel significantly impede magnetic domain wall motion.
  • Micromagnetic simulations provide a reliable tool for interpreting experimental DW dynamics.

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