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Engineering Interfacial Integrity with Hydrolytic-Resistant, Self-Reinforcing Dentin Adhesive.

Erhan Demirel1, Burak Korkmaz1,2, Youngwoo Chang3

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International Journal of Molecular Sciences
|July 13, 2024
PubMed
Summary
This summary is machine-generated.

New dental adhesives using a short-chain silane monomer show improved mechanical strength and reduced degradation. This innovation aims to enhance the longevity of composite restorations by preventing secondary caries.

Keywords:
Raman spectroscopydental adhesivedynamic mechanical analysisinterface studyshort-chain monomersilane monomersol-gel reaction

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Area of Science:

  • Dental Materials Science
  • Polymer Chemistry
  • Biomaterials Engineering

Background:

  • Secondary caries is a primary cause of composite restoration failure.
  • Dental adhesives' susceptibility to damage contributes to restoration failure.
  • Existing silane monomers like γ-methacryloxypropyltrimethoxysilane (MPS) have limitations.

Purpose of the Study:

  • To investigate methacrylate-based resins with methacryloxymethyltrimethoxysilane (MMeS), a short-chain silane alternative.
  • To evaluate the properties of MMeS- and MPS-based dental adhesives.
  • To assess the performance of these adhesives at the adhesive/dentin interface.

Main Methods:

  • Synthesized and characterized methacrylate-based resins with MMeS and MPS.
  • Determined degree of conversion (DC), polymerization kinetics, water sorption, and mechanical properties.
  • Analyzed adhesive/dentin interfaces using chemometrics-assisted micro-Raman spectroscopy.

Main Results:

  • In 30 wt% BisGMA formulations, MMeS-resin showed faster polymerization, lower DC, and reduced leachates compared to MPS-resin.
  • MMeS-resin exhibited enhanced mechanical properties, including increased storage and loss moduli, glass transition temperature (Tg), and crosslink density.
  • Spectroscopic analysis revealed comparable resin-dentin interface integrity across formulations.

Conclusions:

  • The experimental short-chain silane monomer MMeS offers hydrolytic stability and improved mechanical properties in dental adhesives.
  • This autonomous strengthening mechanism enhances material durability.
  • MMeS-based adhesives represent a promising strategy for developing long-lasting restorative dental materials.