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$Microfluidic Chips for In Situ Crystal X-ray Diffraction and In Situ Dynamic Light Scattering for Serial Crystallography$

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Zero-Dimensional Copper(I) Halide Microcrystals as Highly Efficient Scintillators for Flexible X-ray Imaging.

Na Lin^1,2, Xin Wang¹, Hong-Yan Zhang¹

¹Research Institute of Optoelectronic Functional Materials, School of Chemistry, Chemical Engineering and Materials, Jining University, Qufu, Shandong 273155, P. R. China.

ACS Applied Materials & Interfaces

|July 25, 2024

Summary

New zero-dimensional cuprous halides offer highly efficient X-ray detection. These materials enable flexible X-ray imaging with superior performance compared to existing scintillators.

Keywords:

X-ray imaging flexible film metal halides nanomicrocrystals scintillators

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Area of Science:

Materials Science
Radiological Physics
Nanotechnology

Background:

Commercially available X-ray scintillators often suffer from fragility, high detection limits, and demanding preparation conditions.
Developing flexible X-ray imaging technology for complex devices presents significant challenges.

Purpose of the Study:

To synthesize novel, highly efficient, and flexible X-ray scintillators.
To investigate the potential of zero-dimensional (0D) cuprous halides for advanced X-ray imaging applications.

Main Methods:

Synthesis of isostructural cuprous halides: 0D [AEPipz]CuX3·X·H2O (X = Br, I) with controllable size down to the nanoscale.
Characterization of photoluminescence and radioluminescence properties, including quantum yield and light yield.
Fabrication of flexible scintillation films and evaluation of their performance in X-ray imaging.

Main Results:

Synthesized cuprous halides exhibit efficient cyan photoluminescence and radioluminescence with a high quantum yield (92.1%) and light yield (62,400 photons MeV-1).
Achieved an ultralow detection limit of 95.7 nGyair s-1, significantly below diagnostic X-ray doses.
Developed flexible films with excellent foldability and crack resistance, demonstrating high spatial resolution (17.4 lp mm-1) in X-ray imaging.

Conclusions:

The synthesized 0D cuprous halides demonstrate superior X-ray scintillation properties, surpassing commercial materials.
The flexible nature and high performance of these materials make them promising for applications in wearable radiation radiography and flexible X-ray imaging.
These novel cuprous halides represent a significant advancement in the development of next-generation X-ray scintillators.