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Updated: May 10, 2026

Extraction of Lignin with High β-O-4 Content by Mild Ethanol Extraction and Its Effect on the Depolymerization Yield
Published on: January 7, 2019
A green and efficient approach for the simultaneous extraction and mechanisms of essential oil and lignin from
Hongxiang Yang1, Peng Zhou1, Xiangzhou Li2
1College of Materials Science and Engineering, Central South University of Forestry and Technology, Changsha 410004, Hunan, China.
Abstract:
The utilization and economic benefits of biomass resources can be maximized through rational design and process optimization. In this study, an innovative approach for the simultaneous extraction of essential oil and lignin from Cinnamomum camphora leaves by deep eutectic solvent (DES) and optimization of the process parameters was achieved using deep learning tools. With the water content of 40 %, liquid-solid ratio of 9.00 mL/g, and distillation time of 51.81 min, the yields of the essential oil and lignin reached 3.15 ± 0.02 % and 9.75 ± 0.15 %, respectively. Notably, the efficiency of simultaneous extraction of essential oil improved by 23 % compared to that of traditional steam distillation. Moreover, the extraction mechanism of the process was clarified. The connection between lignin with cellulose and hemicellulose was disintegrated by the DES, resulting in lignin shedding and hence accelerating the dissolution of essential oil. Moreover, the compositions of lignin and essential oil were also identified.

