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Updated: Jun 17, 2025

Processing of Bulk Nanocrystalline Metals at the US Army Research Laboratory
Published on: March 7, 2018
Increasing the Strength and Impact Toughness of Carbon Steel Using a Nanosized Eutectoid Resulting from
Michail Brykov1, Dariusz Mierzwiński2, Vasily Efremenko3,4
1Faculty of Engineering and Physics, National University Zaporizhzhia Polytechnic, 69063 Zaporizhzhia, Ukraine.
Abstract:
High-carbon steels are normally used as tool materials. The use of such steels for construction is limited due to their increased brittleness and poor weldability. However, it appears that high-carbon steels possess certain hidden reserves for enhanced plasticity and strength if properly heat-treated. An unconventional heat treatment was applied to carbon eutectoid steel (0.8 wt.% C) in order to increase its strength and impact toughness simultaneously. Samples for tensile and impact testing were held at 800 °C for different time ranges from 3 min to 9 min with subsequent cooling in oil. It was established that for each type of sample, an optimal holding time exists that is responsible for increased strength and high impact toughness. The hardness and microhardness levels of the surface and under-surface regions of the samples reached 390 HV after optimal heat treatment. An X-ray revealed a shift of the (211)α-peak to the lower 2-theta angles after heat treatment with the optimal holding time; this indicates an increase in carbon content in alpha solid solutions of approximately 0.12 wt.%. Thus, a nanostructured mixture of low-carbon martensite and thin cementite plates is formed in the under-surface region of carbon eutectoid steel after heat treatment, with a controlled holding time at the austenitizing temperature.
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