Synthesis of New Complex Ferrite Li_0.5MnFe_1.5O_4: Chemical-Physical and Electrophysical Research

In this article, the sol-gel method was used as a synthesis method, which shows the physicochemical nature of the synthesis of a new complex material, ferrite Li_0.5MnFe_1.5O₄. The structure and composition of the synthesized ferrite were determined by X-ray phase analysis. According to analysis indicators, it was found that our compound is a single-phase, spinel-structured, and syngony-cubic type of compound. The microstructure of the compound and the quantitative composition of the elements contained within it were analyzed under a scanning electron microscope (SEM). Under a scanning electron microscope, microsystems were taken from different parts of Li_0.5MnFe_1.5O₄-type crystallite; the elemental composition of crystals was analyzed; and the general type of surface layer of complex ferrite was shown. As a result, given the fact that the compound consists of a single phase, the clarity of its construction was determined by the topography and chemical composition of the compound. As a result, it was found that the newly synthesized complex ferrites correspond to the formula Li_0.5MnFe_1.5O₄. The particles of the formed compounds have a large size (between 50.0 μm or 20.0 μm and 10.0 μm). Electrophysical measurements were carried out on an LCR-800 unit at intervals of 293-483 K and at frequencies of 1.5 and 10 kHz. An increase in frequency to 10 kHz led to a decrease in the value ε in the range of the studied temperature (293-483 K).