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A flexible rotator-expanded molecular framework integrated strategy for improving microviscosity sensitivity of

Xiaofang Tang1, Yaping Zhu2, Weijiang Guan2

  • 1Pingyuan Laboratory, College of Chemistry, Zhengzhou University, Zhengzhou, 450001, China.

Chemical Communications (Cambridge, England)
|September 6, 2024
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¹H NMR of Conformationally Flexible Molecules: Variable-Temperature NMR01:15

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The axial and equatorial protons in cyclohexane can be distinguished by performing a variable-temperature NMR experiment. In this process, except for one proton, the remaining eleven protons are replaced by deuterium. The deuterium substitution avoids the possible peak splitting caused by the spin-spin coupling between the adjacent protons. The remaining proton flips between the axial and equatorial positions.