Related Experiment Video
Updated: Jun 10, 2025

Chemical Analysis of Water-accommodated Fractions of Crude Oil Spills Using TIMS-FT-ICR MS
Published on: March 3, 2017
Simultaneous measurements of oil- and water-content in crude oil-polluted sands with NMR-deconvolution analysis
Yuxin Wu1, Zihan Zhao1, Hao Ding1
1College of Science, China University of Petroleum, 266580, Qingdao, China. dshw@upc.edu.cn.
Abstract:
This study introduces a novel deconvolution method for accurately quantifying oil or water signals in the NMR spectra of oil-water-sand mixtures. The algorithm employs a parametric model fitting approach that incorporates prior conditions to set parameters. To validate the approach, the widely overlapping NMR spectra of the complex, synthetic oil-water-sand mixes were separated, and their water and oil contents were determined. The results demonstrated high correlation values and maximum errors of 2.11% and 3.90% for water and oil contents, respectively. The proposed deconvolution method provides an innovative solution for simultaneously measuring the content of each fluid in complex porous media containing multiple fluids by NMR spectroscopy and has the potential to facilitate research in the field.
Related Concept Videos
¹³C NMR: ¹H–¹³C Decoupling
A broadband decoupling technique is used to simplify these complex, sometimes overlapping, signals. Broadband decoupling relies on a...
¹H NMR Signal Integration: Overview

