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Preparation and Reactivity of Gasless Nanostructured Energetic Materials
Published on: April 2, 2015
Stable Field Emissions from Zirconium Carbide Nanoneedle Electron Source
Yimeng Wu1,2, Jie Tang1,2, Shuai Tang3
1Research Center for Energy and Environmental Materials, National Institute for Materials Science, Tsukuba 305-0047, Ibaraki, Japan.
Researchers fabricated a single zirconium carbide nanoneedle using focused ion beam-scanning electron microscopy. This nanoneedle demonstrates stable field emission, showing potential as a reliable electron source for advanced devices.
Area of Science:
- Materials Science
- Nanotechnology
- Physics
Background:
- Field emission electron sources are crucial for various electron-beam devices.
- Controlled fabrication of nanostructures is essential for optimizing field emission properties.
Purpose of the Study:
- To fabricate a single zirconium carbide (ZrC) nanoneedle structure.
- To evaluate the field emission characteristics and current stability of the ZrC nanoneedle.
- To demonstrate the potential of ZrC as a field emission emitter.
Main Methods:
- Fabrication of a single ZrC nanoneedle using a dual-beam focused ion beam (FIB-SEM) system.
- Real-time observation for controlled nanostructure fabrication.
- Evaluation of field emission properties in a high-vacuum chamber.
Main Results:
- ZrC nanoneedle with a smooth surface, tip radius < 20 nm, and length > 2 μm.
- Turn-on voltage of 210 V, achieving 100 nA emission current at 325 V.
- Stable emission for 150 min with 1.4% fluctuation and current density of 1.4 × 10^10 A m^-2.
Conclusions:
- An efficient and controllable method for fabricating nanostructures was presented.
- ZrC is a viable material for field emission emitters.
- The fabricated ZrC nanoneedle shows potential as a high-performance electron source for electron-beam devices.
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