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An Available Technique for Preparation of New Cast MnCuNiFeZnAl Alloy with Superior Damping Capacity and High Service Temperature

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Titanium vanadium nickel, TiV_0.08Ni_0.92.

Huizi Liu¹, Changzeng Fan^1,2, Bin Wen¹

¹State Key Laboratory of Metastable Materials Science and Technology Yanshan University,Qinhuangdao 066004 People's Republic of China.

|March 17, 2025

Summary

Researchers synthesized a single crystal of the intermetallic phase titanium-vanadium-nickel (TiVNi) using high-temperature sintering. This compound crystallizes in the CsCl structure type, with specific site occupancies for titanium, vanadium, and nickel.

Keywords:

crystal structure high-pressure sintering intermetallic β phase

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Area of Science:

Materials Science
Solid-State Chemistry
Crystallography

Background:

Intermetallic phases are crucial in materials science for their unique properties.
Understanding crystal structures is fundamental to predicting material behavior.
High-temperature sintering is a common method for synthesizing advanced materials.

Purpose of the Study:

To synthesize and characterize a single crystal of the TiVNi intermetallic phase.
To determine the crystal structure and site occupancy of the synthesized compound.
To contribute to the understanding of phase formation in Ti-V-Ni systems.

Main Methods:

High-temperature sintering of a mixture with nominal composition Ti0.9V0.1Ni.
Single-crystal growth techniques.
X-ray diffraction analysis to determine crystal structure and stoichiometry.

Main Results:

A single crystal of the intermetallic phase TiV0.08Ni0.92 was successfully obtained.
The compound crystallizes in the CsCl structure type.
Detailed site occupancy analysis revealed Ti occupies one site, while V and Ni (ratio 0.08:0.92) occupy the other.

Conclusions:

The synthesis and structural determination of TiV0.08Ni0.92 provide valuable crystallographic data.
The CsCl structure type with specific V/Ni distribution is confirmed for this intermetallic phase.
This study enhances the knowledge of phase formation and crystal chemistry in the titanium-vanadium-nickel system.