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Updated: Sep 19, 2025

Synchrotron X-ray Microdiffraction and Fluorescence Imaging of Mineral and Rock Samples
Published on: June 19, 2018
Reflection grating fabrication for the Rockets for Extended-source X-ray Spectroscopy
Drew M Miles1,2, Ross McCurdy2, Michael Labella3
1Physics, Math, and Astronomy, California Institute of Technology, 1200 E. California Blvd., Pasadena, CA 91125 USA.
Abstract:
The Rockets for Extended-source X-ray Spectroscopy (tREXS) grating spectrograph uses modules of reflection gratings to collect spectroscopic data from extended astronomical sources of soft X-rays. Two blazed master gratings were produced on silicon substrates with electron-beam lithography (EBL) and complementary nanofabrication processes that include KOH etching. Substrate-conformal imprint lithography (SCIL) was then used to create 191 replicas of the two grating masters for use in the flight instrument. Diffraction efficiency was measured for several replica gratings, which achieve a peak of 70% absolute efficiency near 0.22 keV and an average of 50% absolute efficiency across the measured band, from 0.18 - 0.8 keV. Here we detail the nanofabrication of the grating masters, including the EBL parameters and tREXS-specific fabrication considerations, and the SCIL replication process used to generate the final instrument gratings. A discussion of grating characterization and areas for future improvement is also presented.

