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Electrochemical Impedance Spectroscopy as a Tool for Electrochemical Rate Constant Estimation
Published on: October 10, 2018
Protocol for low-cost quantification of microplastics through electrochemical impedance spectroscopy from aqueous
1Department of Civil Engineering, Indian Institute of Technology Delhi, New Delhi 110016, India.
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We present a protocol to quantify microplastics (MPs) in aqueous matrices by analyzing the solution resistance (Rs) imparted by MPs using electrochemical impedance spectroscopy (EIS). We describe steps for preparing the samples, which can provide accurate MP quantification, and detailed steps for configuring the EIS system. We then detail procedures for constructing calibration curves using Rs as the key parameter and validating this technique using ultraviolet-visible spectroscopy. The protocol supports non-destructive, rapid, and low-cost detection of different MP types.

