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X‑ray Micro-Computed Tomography for Structural Analysis of All-Solid-State Battery at Pouch Cell Level.

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Synchrotron X-ray micro-computed tomography (sXCT) non-destructively visualizes all-solid-state battery microstructures. This rapid technique aids in understanding and engineering advanced energy storage systems.

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Area of Science:

  • Materials Science
  • Electrochemistry
  • Battery Technology

Background:

  • Advancing all-solid-state batteries (ASSBs) requires understanding microstructural evolution during fabrication and operation.
  • Scaling ASSBs to pouch cell levels presents challenges for traditional microstructural analysis.

Purpose of the Study:

  • To highlight synchrotron X-ray micro-computed tomography (sXCT) as a powerful tool for characterizing ASSB microstructures.
  • To demonstrate sXCT's capability in analyzing large-scale microstructural features in ASSB pouch cells.

Main Methods:

  • Utilized synchrotron X-ray micro-computed tomography (sXCT) for rapid (<30 min), high-resolution, nondestructive imaging.
  • Analyzed key microstructural features: overhang, porosity, contact loss, active surface area, and tortuosity.
  • Employed a large field of view (up to millimeters) for industry-relevant scale analysis.

Main Results:

  • sXCT effectively visualized and quantified critical microstructural features in all-solid-state pouch cells.
  • Demonstrated the technique's applicability to industry-relevant scales, bridging research and commercialization.
  • Identified potential for integrating sXCT data into multiphysics simulations for degradation analysis.

Conclusions:

  • sXCT is an indispensable tool for advancing the understanding and engineering of next-generation ASSBs.
  • The technique facilitates detailed analysis of microstructural evolution in large-scale ASSB pouch cells.
  • Future integration with simulations can enhance the design of robust and high-performance ASSBs.