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Affordable Automated Modules for Lab-Scale High-Throughput Synthesis of Inorganic Materials.

Iciar Monterrubio1,2, Joseba Orive1, Maha Ismail1,2

  • 1Centre for Cooperative Research on Alternative Energies (CIC energiGUNE), Basque Research and Technology Alliance (BRTA), Alava Technology Park, Albert Einstein 48, Vitoria-Gasteiz, 01510, Spain.

Chemistry (Weinheim an Der Bergstrasse, Germany)
|July 31, 2025
PubMed
Summary
This summary is machine-generated.

Researchers developed a semi-automated station for high-throughput synthesis (HTS) of inorganic materials. This system accelerates materials discovery by enabling efficient screening of compositions and synthesis conditions for applications like Li-ion batteries.

Keywords:
automated synthesis moduleshydrothermal synthesismaterials acceleration platformself‐driven laboratorysol‐gel synthesis

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Area of Science:

  • Materials Science
  • Chemical Engineering
  • Sustainable Materials Development

Background:

  • Growing demand for sustainable, efficient, and scalable research workflows in materials discovery.
  • Advancements in computational screening, high-throughput experimentation (HTE), and artificial intelligence (AI) are key drivers.
  • Materials Acceleration Platforms (MAPs) and Self-Driving Laboratories (SDLs) offer integrated strategies for accelerated research.

Purpose of the Study:

  • To present the development of a semi-automated station for lab-scale high-throughput synthesis (HTS) of inorganic materials.
  • To integrate this system into the Materials Acceleration and Innovation plaTform for ENergy Applications (MAITENA).
  • To demonstrate the system's utility in accelerating materials discovery and property tuning.

Main Methods:

  • Design and implementation of a semi-automated station with two in-house liquid-handling modules.
  • Integration of diverse synthesis techniques: sol-gel, Pechini, solid-state, and hydro/solvothermal.
  • Utilizing the platform for lab-scale HTS of inorganic materials, producing gram-scale samples with reproducibility.

Main Results:

  • The developed station enables high-throughput synthesis of inorganic materials with minimal manual intervention.
  • Each module can prepare dozens of gram-scale samples weekly, ensuring high reproducibility.
  • Case studies using Li-ion battery materials demonstrated efficient screening of compositions and synthesis parameters.

Conclusions:

  • The accessible and modular infrastructure provides a practical approach to implementing HTS in inorganic materials research.
  • The system facilitates rapid screening and optimization of materials for energy applications.
  • This advancement supports the broader goal of accelerating sustainable materials discovery and development.