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Double-Layer Sol-Gel Modifications on Titanium Alloy Substrates-Physicochemical Properties Evaluation.

Katarzyna Matysiak1, Maria Biegun-Żurowska1, Katarzyna Cholewa-Kowalska2

  • 1Department of Ceramics and Refractories, Faculty of Materials Science and Ceramics, AGH University of Krakow, 30-059 Krakow, Poland.

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|August 28, 2025
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Summary

This study developed hybrid coatings using titanium nitride and boron nitride nanoparticles on a medical alloy. These enhanced coatings offer bactericidal properties and protection against surgical wear.

Keywords:
TiAlV alloyTiNhBNhybrid composite layerssol–gel method

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Area of Science:

  • Materials Science
  • Biomedical Engineering
  • Nanotechnology

Background:

  • The TiAlV medical alloy is widely used in implants.
  • There is a need for improved implant coatings with enhanced biocompatibility and durability.
  • Hybrid coatings offer potential for multifunctional surface properties.

Purpose of the Study:

  • To investigate the physicochemical properties of hybrid coatings containing titanium nitride and boron nitride nanoparticles.
  • To assess the suitability of these coatings for medical implants, focusing on bactericidal and anti-abrasion capabilities.
  • To analyze the microstructure, structure, and surface characteristics of the synthesized layers.

Main Methods:

  • Sol-gel process for depositing hybrid coatings on TiAlV alloy.
  • Scanning Electron Microscopy with Energy Dispersive Spectroscopy (SEM + EDS) for microstructural analysis.
  • X-ray Diffraction (XRD) and Fourier-Transform Infrared Spectroscopy (FTIR) for structural characterization.
  • Contact angle measurements for wettability, surface free energy, and roughness analysis.

Main Results:

  • Successful fabrication of hybrid layers with varied microstructures and morphologies.
  • FTIR and XRD analyses confirmed the incorporation of titanium nitride and boron nitride nanoparticles within an organosilicon matrix.
  • Surface property evaluations indicated potential for improved implant performance.

Conclusions:

  • The sol-gel process is effective for creating hybrid coatings with titanium nitride and boron nitride nanoparticles on TiAlV alloy.
  • The developed coatings exhibit promising characteristics for enhancing implant functionality, including bactericidal effects and wear resistance.
  • Further research can explore optimizing these coatings for specific clinical applications.