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Structure-Tunable Fluorinated Polyester Electrolytes with Enhanced Interfacial Stability for Recyclable Solid-State

Xinke Dai1,2, Hai-Mu Ye1, Guoyong Huang1

  • 1College of New Energy and Materials, State Key Laboratory of Heavy Oil Processing, China University of Petroleum, Beijing, 102249, China.

Advanced Materials (Deerfield Beach, Fla.)
|September 8, 2025
PubMed
Summary

Fluorinated polyesters show promise for solid-state lithium metal batteries. Molecular design and recycling strategies enhance ionic conductivity and sustainability for advanced energy storage.

Keywords:
battery recyclingfluorinated polyesterinterface stabilitylithium metal batterysolid‐state electrolyte

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Area of Science:

  • Materials Science
  • Electrochemistry
  • Polymer Chemistry

Background:

  • Polyesters are gaining attention as sustainable solid polymer electrolytes for solid-state lithium metal batteries (SSLMBs).
  • Tuning polyester structure is key to optimizing performance in battery applications.

Purpose of the Study:

  • To investigate the impact of systematic fluorination on polyester structure and ionic conductivity.
  • To develop a cost-effective and sustainable recycling method for fluorinated polyester electrolytes.

Main Methods:

  • Fabrication of 18 polyester types with varied carbon chain lengths and fluorination positions.
  • Experimental and theoretical studies to analyze ionic conductivity, crystallinity, and interfacial stability.
  • Development and evaluation of a solvent-based recycling process.

Main Results:

  • Fluorination at the coordinating segment enhanced ionic conductivity by reducing crystallinity.
  • Fluorination at the flexible segment improved lithium-ion transference number by creating homogeneous coordinating sites.
  • Optimized polyesters demonstrated excellent interfacial stability with lithium metal, forming a LiF-rich interphase.
  • A solvent-based recycling route achieved high recovery yields and environmental benefits.

Conclusions:

  • Molecular design of fluorinated polyesters offers a versatile strategy for enhancing SSLMB performance.
  • The developed closed-loop recovery strategy promotes cost-effectiveness and sustainability.
  • These advancements pave the way for practical applications of high-energy and sustainable SSLMBs.