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Related Concept Videos

Precipitation Gravimetry01:03

Precipitation Gravimetry

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Precipitation gravimetry is based on converting an analyte into a sparingly soluble precipitate, which is separated by filtration and weighed. An ideal precipitate should be pure, insoluble, of known composition, and easily filtered from the reaction mixture.
In determining nickel by gravimetric analysis, a precipitant of ethanolic dimethylglyoxime is added to a hot nickel salt solution. This is quickly followed by the dropwise addition of dilute ammonia solution until precipitation occurs. A...
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Washing, Drying, and Ignition of Precipitates00:52

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After filtration, the precipitate is washed to remove coprecipitated impurities and any remaining mother liquor. Colloidal precipitates, such as silver chloride, are washed with an electrolyte (such as dilute nitric acid) to prevent the peptization of the precipitate. In the case of slightly soluble precipitates, the wash solution contains a common ion to reduce solubility. Lead sulfate, which is slightly soluble in water, is washed with dilute sulfuric acid. Similarly, wash solutions may be...
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Processing of Bulk Nanocrystalline Metals at the US Army Research Laboratory
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Cold-Sprayed Ni and NdFeB-Al Powders Recovery and Reuse.

Jean-Michel Lamarre1, Alexandre Nascimento2, Cindy Charbonneau1

  • 1National Research Council Canada, 75 Boul. de Mortagne, Boucherville, QC J4B 6Y4, Canada.

Materials (Basel, Switzerland)
|November 13, 2025
PubMed
Summary

Recovering and reusing cold spray powders, like nickel and NdFeB-Al, improves process economics. Even after multiple cycles, recovered powders maintain their performance for additive manufacturing applications.

Keywords:
NdFeBNickelcold spraymagnetspowder recoverysustainability

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Area of Science:

  • Materials Science
  • Additive Manufacturing
  • Powder Metallurgy

Background:

  • Cold spray additive manufacturing faces challenges with low deposition efficiency for certain materials, leading to feedstock waste.
  • Economically viable mass production and use of expensive materials necessitate solutions to powder waste.

Purpose of the Study:

  • To investigate the feasibility and impact of powder recovery and reuse in cold spray processes.
  • To evaluate the effect of recovery on powder characteristics and coating performance for Ni and NdFeB-Al powders.

Main Methods:

  • Development and testing of a prototype powder recovery system.
  • Characterization of recovered powder morphology and size distribution after multiple spray runs.
  • Evaluation of magnetic properties of powders and coatings using hysteresis measurements.

Main Results:

  • The prototype recovery system achieved up to 75% recovery efficiency.
  • Recovered Ni and NdFeB-Al powders, even after four spray runs, remained suitable for re-deposition.
  • NdFeB-Al powder retained 97% of its initial magnetic performance under industrial conditions.

Conclusions:

  • Powder recovery and reuse is a viable strategy to improve the economics of cold spray additive manufacturing.
  • Despite minor alterations in particle size and magnetic properties, recovered powders maintain performance for repair and permanent magnet fabrication.