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Solid-state Graft Copolymer Electrolytes for Lithium Battery Applications
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Zeolite β-Hydrogen Composite Polymer Electrolyte for Enhanced Lithium Anode Performance.

Layla Khayat1, Md Yasir Bhat2, Firoz Khan1,2

  • 1Material Science and Engineering Department, King Fahd University of Petroleum & Minerals (KFUPM), Dhahran, Saudi Arabia.

Chemistry, an Asian Journal
|November 14, 2025
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Summary

A novel composite polymer electrolyte (CPE) with zeolite filler enhances solid polymer electrolyte performance for all-solid-state lithium metal batteries. This material shows improved ionic conductivity and stability, enabling durable battery applications.

Keywords:
all‐solid‐state lithium metal batteriescomposite polymer electrolytelong cycling capabilitystable interfacezeolite fillers

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Area of Science:

  • Materials Science
  • Electrochemistry
  • Polymer Science

Background:

  • Solid polymer electrolytes (SPEs) face challenges like unstable interfaces with lithium anodes and low ionic conductivity, hindering their use in all-solid-state lithium metal batteries (ALMBs).
  • Polyethylene oxide (PEO)-based SPEs are particularly limited by these issues.
  • Composite polymer electrolytes (CPEs) offer a potential solution by incorporating fillers to improve properties.

Purpose of the Study:

  • To develop a composite polymer electrolyte (CPE) using zeolite filler to overcome the limitations of traditional SPEs for ALMBs.
  • To investigate the electrochemical properties and anode compatibility of the synthesized CPE.
  • To assess the potential of the new CPE for high-performance and durable ALMBs.

Main Methods:

  • Synthesis of a composite polymer electrolyte (CPE) incorporating zeolite β-hydrogen (H-BEA) filler, termed CPE-H.
  • Measurement of ionic conductivity and Li-ion transference number of CPE-H at 60°C.
  • Galvanostatic lithium plating and stripping (GLPS) tests at various current densities to evaluate overpotential and cycling stability.

Main Results:

  • CPE-H exhibited an ionic conductivity of approximately 4.37 × 10-4 S cm-1 at 60°C.
  • A Li-ion transference number of approximately 0.62 was achieved with CPE-H.
  • Low overpotentials (8-58 mV) were observed across current densities from 50 to 300 µA cm-2, with excellent Li anode compatibility over 2000 hours at 100 µA cm-2.

Conclusions:

  • The synthesized CPE-H demonstrates significantly improved ionic conductivity and Li-ion transference number compared to conventional SPEs.
  • CPE-H exhibits excellent stability and compatibility with Li anodes, as evidenced by low overpotentials and long-term cycling performance.
  • This zeolite-filled CPE holds considerable promise for the development of high-performance and durable all-solid-state lithium metal batteries.