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Garnet-Type Solid-State Electrolyte with Tailored Lithium Compatibility for High Performance All-Solid-State Lithium

Yang Zhang1, Shuhan Wang1, Kai Wan2

  • 1College of Materials and Chemistry & Chemical Engineering, Chengdu University of Technology, Chengdu, 610059, P. R. China.

Advanced Materials (Deerfield Beach, Fla.)
|December 10, 2025
PubMed
Summary
This summary is machine-generated.

This study developed new garnet solid-state electrolytes (LLZSOF) with improved lithium metal compatibility. These electrolytes show excellent performance in all-solid-state batteries, paving the way for scalable applications.

Keywords:
all‐solid‐state lithium batteriesgarnet‐type solid electrolytesinterfacial contactreduction stability

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Area of Science:

  • Materials Science
  • Electrochemistry
  • Solid-State Chemistry

Background:

  • Garnet-type Li7La3Zr2O12 (LLZO) solid-state electrolytes (SSEs) offer high ionic conductivity for all-solid-state batteries.
  • Interfacial compatibility between LLZO and lithium metal electrodes remains a challenge for practical battery deployment.

Purpose of the Study:

  • To design and synthesize novel garnet-type SSEs (Li7La3Zr2-xScxO12-xFx, LLZSOF) with enhanced lithium metal compatibility.
  • To investigate the effect of scandium and fluorine doping on the structural, electrochemical, and interfacial properties of LLZO.

Main Methods:

  • Synthesis of LLZSOF materials with varying Sc and F content (x = 0-0.20).
  • Characterization of crystal structure, ionic conductivity, and electrochemical stability.
  • Fabrication and testing of symmetric cells and all-solid-state lithium metal batteries (ASLMBs).

Main Results:

  • Optimized LLZSOF-0.15 composition demonstrated strong interfacial contact with lithium metal, inhibiting Li+/H+ exchange.
  • Scandium substitution increased lithium content and improved reduction stability.
  • LLZSOF-0.15 based symmetric cells achieved a critical current density of 1.9 mA cm-2.
  • ASLMBs using LLZSOF-0.15 exhibited excellent cyclability with high capacity retention for LiFePO4 and NCM cathodes.
  • Pouch cells demonstrated high Coulombic efficiency (>99.5%) and capacity retention (>94.9%) over 120 cycles.

Conclusions:

  • The developed LLZSOF SSEs exhibit superior interfacial compatibility with lithium metal electrodes.
  • This material design approach promotes the development of advanced garnet SSEs for scalable all-solid-state battery applications.