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Related Concept Videos

Precipitate Formation and Particle Size Control01:16

Precipitate Formation and Particle Size Control

In precipitation gravimetry, the precipitating agent should react specifically or selectively with the analyte. While a specific reagent reacts with the analyte alone, a selective reagent can react with a limited number of chemical species.
The obtained precipitate should be either a pure substance of known composition or easily converted to one by a simple process, such as ignition or drying. In addition, the precipitate should be insoluble and easily filterable. In general, filterability...
Colloidal precipitates01:09

Colloidal precipitates

The high insolubility of some precipitates can result in an unfavorable relative supersaturation. This can lead to colloidal particles with a large surface-to-mass ratio, where adsorption is promoted. For instance, in the precipitation of silver chloride, silver ions are adsorbed on the surface of the colloidal particles, forming a primary layer. This layer attracts ions of opposite charge (such as nitrate ions), forming a diffuse secondary layer of adsorbed ions. This electric double layer...
Washing, Drying, and Ignition of Precipitates00:52

Washing, Drying, and Ignition of Precipitates

After filtration, the precipitate is washed to remove coprecipitated impurities and any remaining mother liquor. Colloidal precipitates, such as silver chloride, are washed with an electrolyte (such as dilute nitric acid) to prevent the peptization of the precipitate. In the case of slightly soluble precipitates, the wash solution contains a common ion to reduce solubility. Lead sulfate, which is slightly soluble in water, is washed with dilute sulfuric acid. Similarly, wash solutions may be...

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Tailoring Sulfide Particle Size for All-Solid-State Lithium Metal Batteries.

Ziqi Zhang1, Changqing Jing2, Jingming Yao3

  • 1Key Laboratory for Renewable Energy, Beijing Key Laboratory for New Energy Materials and Devices, Beijing National Laboratory for Condensed Matter Physics, Institute of Physics, Chinese Academy of Sciences, Beijing, China.

Advanced Materials (Deerfield Beach, Fla.)
|January 9, 2026
PubMed
Summary
This summary is machine-generated.

Optimizing sulfide solid electrolyte (SSE) particle size in all-solid-state lithium metal batteries (ASSLBs) enhances ion conduction. Controlled grinding and specific particle size ratios (D50, D90) yield superior capacity, rate capability, and cyclability.

Keywords:
Li metal anodeNi‐rich cathodeall‐solid‐state batteryargyroditeparticle sizesulfide solid electrolyte

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Area of Science:

  • Materials Science
  • Electrochemistry
  • Battery Technology

Background:

  • Precise control of sulfide solid electrolyte (SSE) particle size is critical for efficient ion-conducting networks in composite cathodes.
  • All-solid-state lithium metal batteries (ASSLBs) require optimized SSE for improved performance.

Purpose of the Study:

  • To systematically investigate the impact of SSE particle size distribution (D10, D50, D90) on ASSLB performance.
  • To establish quantitative guiding principles for SSE particle engineering in composite cathodes.

Main Methods:

  • Controlled mechanical grinding of Li6PS5Cl SSE to achieve specific particle size distributions.
  • Electrochemical testing (capacity, rate capability, cyclability) of ASSLBs with varying SSE particle sizes.
  • Microstructural analysis to correlate particle configuration with ion-conducting network formation.

Main Results:

  • Optimal SSE particle size composition resulted in a reversible capacity of 202.2 mAh/g at 0.25C.
  • Superior rate capability (76% capacity retention at 5C/0.25C) and cyclability (80% at 5C after 4000 cycles) were achieved.
  • A hierarchical ion-conducting network formed under specific cathode-to-SSE particle size ratios (7.3 ≤ D50Cathode/D50SSE and 2.0 ≤ D90Cathode/D90SSE ≤ 3.5).

Conclusions:

  • Optimized SSE particle size engineering is crucial for high-performance ASSLBs.
  • Fine SSE particles fill cathode gaps, while medium particles facilitate ion transport.
  • Deviations in particle size ratios negatively impact interfacial contact and ion transport pathways.