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From experimental data to thermophysical insight: characterizing choline-based ionic liquids using advanced data

Mahasoa-Salina Souvenir-Zafindrajaona1,2,3, Jean-Pierre Mbakidi2, Zdeněk Wagner3

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This study investigates how water content affects choline-based ionic liquids (CHILs) used for biomass processing. Hydration significantly alters their thermophysical properties, crucial for efficient lignin dissolution and green chemistry applications.

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Area of Science:

  • Green Chemistry
  • Materials Science
  • Chemical Engineering

Background:

  • Efficient extraction of compounds from biomass necessitates effective dissolution methods.
  • Choline-based ionic liquids (CHILs) have demonstrated efficacy in dissolving lignin.
  • Understanding the influence of hydration on CHIL properties is key for optimizing biomass processing.

Purpose of the Study:

  • To investigate the impact of hydration on the thermophysical properties of four CHILs.
  • To determine how water content modulates the performance of CHILs in biomass dissolution.
  • To advance the fundamental understanding of CHIL-water mixtures for sustainable applications.

Main Methods:

  • Measurement of density and isobaric heat capacity of CHILs at various temperatures and hydration levels.
  • Careful control of water content and extrapolation to zero water content to obtain pure-phase properties.
  • Application of a robust non-statistical approach based on mathematical gnostics for data analysis, including uncertainty and outlier detection.

Main Results:

  • Derived apparent molar properties revealed distinct ion-water interactions in CHIL-water mixtures.
  • Hydration was shown to significantly modulate the thermophysical properties of the studied CHILs.
  • The study successfully derived pure-phase properties of CHILs by controlling and extrapolating water content.

Conclusions:

  • Hydration plays a critical role in tuning the performance of CHILs for biomass processing.
  • The findings provide fundamental insights into CHIL-water interactions.
  • This research supports the development of CHILs for sustainable biomass processing and green chemical technologies.