Jove
Visualize
Contact Us
JoVE
x logofacebook logolinkedin logoyoutube logo
ABOUT JoVE
OverviewLeadershipBlogJoVE Help Center
AUTHORS
Publishing ProcessEditorial BoardScope & PoliciesPeer ReviewFAQSubmit
LIBRARIANS
TestimonialsSubscriptionsAccessResourcesLibrary Advisory BoardFAQ
RESEARCH
JoVE JournalMethods CollectionsJoVE Encyclopedia of ExperimentsArchive
EDUCATION
JoVE CoreJoVE BusinessJoVE Science EducationJoVE Lab ManualFaculty Resource CenterFaculty Site
Terms & Conditions of Use
Privacy Policy
Policies

Related Concept Videos

Quantum Numbers02:43

Quantum Numbers

39.9K
It is said that the energy of an electron in an atom is quantized; that is, it can be equal only to certain specific values and can jump from one energy level to another but not transition smoothly or stay between these levels.
39.9K
Electronic Structure of Atoms02:28

Electronic Structure of Atoms

21.7K

An atom comprises protons and neutrons, which are contained inside the dense, central core called the nucleus, with electrons present around the nucleus. Taking into account the wave–particle duality of electrons and the uncertainty in position around the nucleus, quantum mechanics provides a more accurate model for the atomic structure. It describes atomic orbitals as the regions around the nucleus where electrons of discrete energy exist, characterized by four quantum...
21.7K
Mass Spectrum01:23

Mass Spectrum

5.3K
A mass spectrum is the graphical representation of the relative abundance of the charged fragments in an analyte plotted against their mass-to-charge ratio (m/z). The plot's x-axis represents the ratio of the mass of the charged fragment to the number of charges it carries. The y axis of the plot represents the relative abundance of each charged species. The relative abundance is calculated from the signal intensity of each charged species recorded at the detector. The most intense signal (the...
5.3K
Interpreting ¹H NMR Signal Splitting: The (n + 1) Rule01:10

Interpreting ¹H NMR Signal Splitting: The (n + 1) Rule

2.9K
In the AX proton spin system, proton A can sense the two spin states of a coupled proton X, resulting in a doublet NMR signal with two peaks of equal (1:1) intensity. When proton A is coupled to two equivalent protons (AX2 spin system), the spin states of each X can be aligned with or against the external field, creating three possible scenarios. This results in a 1:2:1  triplet signal, where the central peak corresponds to the chemical shift of A and is twice as large or intense as the...
2.9K
MALDI-TOF Mass Spectrometry01:19

MALDI-TOF Mass Spectrometry

5.8K
Mass spectrometry is a powerful characterization technique that can identify and separate a wide variety of compounds ranging from chemical to biological entities, based on their mass-to-charge ratio (m/z). The instruments that allow this detection, known as mass spectrometers, have three components: an ion source, a mass analyzer, and a detector. These spectrometers differ based on the nature of their ion source and analyzers.Matrix-assisted laser desorption ionization (MALDI) is a commonly...
5.8K
Mass Spectrum: Interpretation01:24

Mass Spectrum: Interpretation

4.1K
An unknown compound can be established by identifying the molecular ion peak in the mass spectrum. The molecular ion peak is often weak or absent due to the predominance of fragmentation in high-energy electron beams. In such cases, a soft-energy electron beam can be used to scan the spectrum to enhance the intensity of the molecular ion peak. Additionally, chemical ionization, field ionization, and desorption ionization spectra are used to obtain a relatively intense molecular ion peak.To...
4.1K

You might also read

Related Articles

Articles linked to this work by shared authors, journal, and citation graph.

Sort by
Same author

The matrix pencil as a tunable filter.

Journal of magnetic resonance (San Diego, Calif. : 1997)·2024
Same author

Data processing in NMR relaxometry using the matrix pencil.

Journal of magnetic resonance (San Diego, Calif. : 1997)·2020
Same author

Experimental estimates of compression heating and decompression cooling in ethylene glycol.

Magnetic resonance in chemistry : MRC·2019
Same author

Analytical approximations to inhomogeneously broadened, radiation damped free precession and echo signals.

Journal of magnetic resonance (San Diego, Calif. : 1997)·2013
Same author

A single coil radio frequency gradient probe for nuclear magnetic resonance applications.

The Review of scientific instruments·2013
Same author

Application of bivariate statistics to full wine bottle diamagnetic screening data.

Talanta·2012
Same journal

Experimental and computational <sup>11</sup>B NMR comparative study of MOVPE-grown rhombohedral and bulk hexagonal boron nitride.

Solid state nuclear magnetic resonance·2026
Same journal

Determination of <sup>137</sup>Ba nuclear quadrupole interactions in solids: a comparison of high field and zero field approaches.

Solid state nuclear magnetic resonance·2026
Same journal

Probing interlayer bromide in solvent intercalation of layered yttrium hydroxide via <sup>79/81</sup>Br SSNMR spectroscopy.

Solid state nuclear magnetic resonance·2026
Same journal

Single crystal sapphire spacers for in situ angle sensing and rotor stability diagnostics in MAS NMR.

Solid state nuclear magnetic resonance·2026
Same journal

Insights into the local adsorption of CO<sub>2</sub> in UiO-66.

Solid state nuclear magnetic resonance·2026
Same journal

<sup>75</sup>As NQR characterisation of cobaltite (CoAsS).

Solid state nuclear magnetic resonance·2026
See all related articles

Related Experiment Video

Updated: May 6, 2026

Atomic Scale Structural Studies of Macromolecular Assemblies by Solid-state Nuclear Magnetic Resonance Spectroscopy
14:55

Atomic Scale Structural Studies of Macromolecular Assemblies by Solid-state Nuclear Magnetic Resonance Spectroscopy

Published on: September 17, 2017

16.8K

(MAS)n, n ≤ 8.

A J Soukey1, M P Augustine2

  • 1ACME, 3925 E. Midas Ave., Rocklin, CA, 95677, USA.

Solid State Nuclear Magnetic Resonance
|March 17, 2026
PubMed
Summary
This summary is machine-generated.

This study introduces a low-cost, 3D-printed magic angle spinning (MAS) stator for solid-state nuclear magnetic resonance (NMR) spectroscopy. This innovation enables simultaneous spinning of multiple samples, enhancing signal intensity and accessibility for researchers.

Keywords:
BenchtopMASMagic angle spinning

More Related Videos

Cryogenic Sample Loading into a Magic Angle Spinning Nuclear Magnetic Resonance Spectrometer that Preserves Cellular Viability
06:42

Cryogenic Sample Loading into a Magic Angle Spinning Nuclear Magnetic Resonance Spectrometer that Preserves Cellular Viability

Published on: September 1, 2020

2.8K
High-Temperature and High-Pressure In situ Magic Angle Spinning Nuclear Magnetic Resonance Spectroscopy
08:55

High-Temperature and High-Pressure In situ Magic Angle Spinning Nuclear Magnetic Resonance Spectroscopy

Published on: October 9, 2020

4.7K

Related Experiment Videos

Last Updated: May 6, 2026

Atomic Scale Structural Studies of Macromolecular Assemblies by Solid-state Nuclear Magnetic Resonance Spectroscopy
14:55

Atomic Scale Structural Studies of Macromolecular Assemblies by Solid-state Nuclear Magnetic Resonance Spectroscopy

Published on: September 17, 2017

16.8K
Cryogenic Sample Loading into a Magic Angle Spinning Nuclear Magnetic Resonance Spectrometer that Preserves Cellular Viability
06:42

Cryogenic Sample Loading into a Magic Angle Spinning Nuclear Magnetic Resonance Spectrometer that Preserves Cellular Viability

Published on: September 1, 2020

2.8K
High-Temperature and High-Pressure In situ Magic Angle Spinning Nuclear Magnetic Resonance Spectroscopy
08:55

High-Temperature and High-Pressure In situ Magic Angle Spinning Nuclear Magnetic Resonance Spectroscopy

Published on: October 9, 2020

4.7K

Area of Science:

  • Materials Science
  • Analytical Chemistry
  • Spectroscopy

Background:

  • Solid-state magic angle spinning (MAS) nuclear magnetic resonance (NMR) is a powerful technique for characterizing solid materials.
  • Traditional MAS NMR requires specialized and often expensive equipment, limiting its accessibility.

Purpose of the Study:

  • To develop and demonstrate a low-cost, 3D-printable MAS stator for benchtop NMR magnets.
  • To enable simultaneous spinning of multiple solid samples within a single NMR probe.
  • To reduce the cost barrier for solid-state MAS NMR applications.

Main Methods:

  • 3D printing of a novel MAS stator design capable of holding multiple rotors.
  • Experimental setup utilizing a benchtop magnet and standard NMR probe.
  • Acquisition of 79Br NMR spectra for single and multiple powdered solid samples (KBr, NaBr).

Main Results:

  • Stable spinning of powdered solid samples in 4 mm rotors up to 7 kHz achieved.
  • Demonstrated increase in signal-to-noise ratio by simultaneously spinning multiple samples of the same material.
  • Successful execution of mixed-sample studies using rotors with different materials (KBr and NaBr).
  • A stator design for spinning up to 8 samples simultaneously was presented.

Conclusions:

  • The 3D-printed MAS stator significantly lowers the cost and complexity of solid-state MAS NMR.
  • Simultaneous multi-sample spinning enhances experimental efficiency and signal detection.
  • This technology democratizes access to solid-state MAS NMR for broader research communities.