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Updated: Mar 29, 2026

Untargeted Liquid Chromatography-Mass Spectrometry-Based Metabolomics Analysis of Wheat Grain
Published on: March 13, 2020
Semi-Quantitative Detection of Borax Adulteration in Wheat Flour Based on Microwave Non-Destructive Testing and
Mei Kang1, Jiming Yang1, Ya Ren2
1School of Electrical and Information Engineering, Jiangsu University, Zhenjiang 212013, China.
Abstract:
The adulteration of wheat flour with borax poses a serious food safety risk, yet conventional rapid non-destructive screening methods remain limited. This study developed a machine learning-based microwave non-destructive semi-quantitative detection method for identifying borax adulteration in wheat flour. Using a proprietary microwave detection system, which acquires broadband frequency-domain amplitude attenuation and phase shift responses in the 2.5-11.5 GHz band, amplitude attenuation spectra and dimensional phase offset spectra were obtained from 155 samples prepared at three adulteration levels (0%, 0.1-0.9%, 1-5%). These samples simulated real-world adulteration scenarios. To address high-dimensionality and class imbalance, a hybrid Random Forest-Whale Optimization Algorithm (RF-WOA) was employed to synergistically optimize feature selection and model hyperparameters. Through hierarchical repeated validation and macro-level metric evaluation, this approach achieved an overall classification accuracy of 94.6% and a macro F1 score of 0.95 while compressing the original 1800-dimensional feature space to approximately 200 effective features. Confusion matrix analysis indicates 100% recall for undiluted samples, with misclassifications primarily occurring between adjacent adulteration levels and no false negatives introduced for adulterated samples. These results demonstrate that microwave sensing combined with the RF-WOA provides a rapid, non-destructive, and robust preliminary screening and grading evaluation strategy for borax adulteration in wheat flour, exhibiting significant potential in food safety monitoring and regulatory inspection.
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