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Updated: Jun 29, 2026

Cryo-electron Microscopy Specimen Preparation By Means Of a Focused Ion Beam
Published on: July 26, 2014
Cryogenic etching device based on the conductive cooling method using liquid nitrogen bath
Kil-Byoung Chai1,2, Eun-Beom Choi3, Hyo-Chang Lee3
1Nuclear Physics Application Research Division, Korea Atomic Energy Research Institute, Daejoen 34057, Republic of Korea.
Abstract:
We developed a cryogenic etching device capable of precise temperature control utilizing liquid nitrogen conductive cooling. This device achieves electrode temperatures as low as -170 °C and enables real-time electrode temperature control, providing a reliable alternative to existing cryogenic etching techniques. To demonstrate the performance of our device, we conducted etching experiments on trench-patterned SiO2 thin films, successfully achieving anisotropic etching under cryogenic conditions. Compared with conventional methods such as flowing liquid nitrogen and chillers, our apparatus has a simple electrode structure, eliminates the risk of coolant leakage, and enables real-time temperature control. With these advantages, it is expected that our device based on the liquid nitrogen conductive cooling can be widely used in cryogenic etching research.
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