Related Experiment Video
Updated: Apr 8, 2026

Experimental and Data Analysis Workflow for Soft Matter Nanoindentation
Published on: January 18, 2022
Automation of nanoindentation targeting control using machine vision
Vivek Chawla1, Dayakar Penumadu1, Sergei Kalinin2
1Department of Civil and Environmental Engineering, University of Tennessee, Knoxville, Tennessee 37996, USA.
This study introduces an automated nanoindentation framework for precise mechanical property testing. It enables efficient, targeted characterization of complex materials, paving the way for autonomous testing.
Area of Science:
- Materials Science
- Mechanical Engineering
- Nanotechnology
Background:
- Nanoindentation is crucial for nanoscale mechanical property evaluation.
- Conventional methods struggle with targeted analysis of microstructural features.
- A need exists for automated, precise nanoindentation workflows.
Purpose of the Study:
- To develop an automated nanoindentation framework supporting machine learning.
- To enhance precision and efficiency in characterizing complex materials.
- To enable feature-based and large-scale automated indentation.
Main Methods:
- Implemented a three-mode automated system: standard, feature-based (image-to-coordinate mapping), and large-scale.
- Utilized direct sample-to-indenter alignment to minimize travel errors.
- Employed pixel-to-micron calibration for accurate navigation and Self-Organizing Feature Maps for guided indentation.
Main Results:
- Achieved precise, automated indentation with reduced user intervention.
- Demonstrated phase-specific and orientation-guided indentation capabilities.
- Mitigated initial travel-distance errors by 2.5-6 μm through direct alignment.
Conclusions:
- The developed framework significantly enhances precision and efficiency in nanoindentation.
- It enables targeted characterization of microstructurally complex materials.
- The adaptable interface supports integration with existing nanoindenter platforms for autonomous testing.
More Related Videos
10:06Characterization Of Multi-layered Fish Scales Atractosteus spatula Using Nanoindentation, X-ray CT, FTIR, and SEM
Published on: July 10, 2014
08:58Atomic Force Microscopy Cantilever-Based Nanoindentation: Mechanical Property Measurements at the Nanoscale in Air and Fluid
Published on: December 2, 2022