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Updated: May 5, 2026

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Synchrotron X-ray Microdiffraction and Fluorescence Imaging of Mineral and Rock Samples
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Non-Destructive Quantitative Characterization of Constituent Content in C/C-SiC Composites Based on Multispectral
Xin Yan1,2, Kai He2, Guilong Gao2
1School of Missile Engineering, Rocket Force University of Engineering, Xi'an 710025, China.
Sensors (Basel, Switzerland)
|May 4, 2026
Summary
This study introduces a physics-guided framework using multispectral photon-counting X-ray detection for non-destructive analysis of C/C-SiC composites. The method accurately quantifies silicon carbide (SiC) mass fraction, crucial for quality control.
Area of Science:
- Materials Science
- Physics
- Engineering
Background:
- Non-destructive quantitative characterization of constituent content in C/C-SiC composites is challenging.
- Photon-counting X-ray measurements are affected by detector non-idealities and beam-hardening effects.
Purpose of the Study:
- To develop a physics-guided framework for accurate, non-destructive constituent content characterization in C/C-SiC composites.
- To address distortions in multispectral attenuation features caused by detector response and polychromatic X-ray sources.
Main Methods:
- A Geant4 11.2-based detector-response model was integrated into a unified correction workflow.
- Beam-hardening compensation was applied to recover physically consistent multispectral attenuation vectors.
- A theoretical database of SiC mass fractions was established for constituent inversion.
Main Results:
- The framework effectively suppresses thickness-dependent bias in attenuation measurements.
- An average relative error below 3% was achieved for pure aluminum.
- SiC mass fraction in C/C-SiC composites was quantified with accuracy better than 3 wt%.
Conclusions:
- The proposed method offers a practical non-destructive route for characterizing heterogeneous ceramic-matrix composites.
- This technique is valuable for manufacturing quality control and in-service assessment of C/C-SiC materials.
Keywords:
C/C–SiC compositesconstituent inversioneffective atomic number (Zeff)multispectral X-ray detectionnon-destructive characterizationphoton-counting detector (PCD)More Related Videos
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