Mechanisms of Microstructural and Defect Evolution in Laser Powder Bed Fusion-Fabricated In625 Induced by Heat...

Heat treatment is essential for In625 fabricated by laser powder bed fusion (L-PBF), as it significantly influences microstructural evolution, defect behavior, and mechanical performance. In this study, the effects of different solution heat treatments on L-PBF-fabricated In625 were systematically investigated. Industrial computed tomography was employed to characterize internal defects before and after heat treatment, while optical microscopy, EBSD, TEM, and EDS were used to analyze microstructural evolution. Room-temperature tensile tests evaluated mechanical properties. The results show that heat treatment at 1090 °C reduces porosity from 0.33% to 0.25%, whereas increasing the temperature to 1150 °C results in a further increase in porosity to 0.45%. This non-monotonic behavior is interpreted as the result of competing mechanisms, including partial closure of small pores at 1090 °C and pore coarsening/enlargement at higher temperatures, with the latter possibly involving the growth of sub-resolution pores into the CT-detectable range. Complete grain equiaxiality occurs after heat treatment at 1090 °C or higher, with average grain sizes below 100 μm, although grain coarsening becomes pronounced at higher temperatures. Samples heat-treated at 1150 °C exhibit reduced mechanical anisotropy, achieving tensile strength above 919 MPa and elongation up to 60%. These results clarify the mechanisms by which heat treatment governs microstructure-defect-property relationships in L-PBF In625, guiding its engineering application.