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Quantitative Imaging Method of Metallic Lithium Surface Density Using Muonic X-rays.

S Takeda1,2,3, M Katsuragawa2,4, T Takahashi2,5

  • 1Fukushima Institute for Research, Education and Innovation (F-REI), 6-1 Yazawa-machi, Gongendo, Namie, Namie, Fukushima 979-1521, Japan.

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Researchers developed a new imaging system for muonic X-ray spectroscopy (μXRS) to quantitatively map lithium deposition on battery anodes. This breakthrough enables non-destructive, 2D imaging of lithium, crucial for battery safety and performance analysis.

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Area of Science:

  • Materials Science
  • Analytical Chemistry
  • Physics

Background:

  • Quantitative and nondestructive detection of metallic lithium deposition on Li-ion battery anodes is crucial for understanding degradation and ensuring safety.
  • Muonic X-ray spectroscopy (μXRS) is sensitive to light elements like lithium and can probe bulk materials.
  • Conventional μXRS detectors lack the spatial resolution needed for practical device analysis.

Purpose of the Study:

  • To develop a novel imaging system for spatially resolved quantification of metallic lithium deposition using μXRS.
  • To demonstrate the capability of the new system for 2D imaging of lithium surface density.
  • To establish μXRS as a viable non-destructive diagnostic tool for battery safety inspection.

Main Methods:

  • Development of a novel μXRS imaging system incorporating a large-area silicon double-sided strip detector and a 3D-printed tungsten parallel-hole collimator.
  • Quantitative 2D imaging of metallic lithium surface density using Li plate samples.
  • Application of an original image-processing algorithm to suppress crosstalk and correct beam profiles for accurate quantification.

Main Results:

  • Demonstrated the first quantitative 2D imaging of metallic lithium surface density with a spatial resolution of 5 mm.
  • Achieved a 1-σ detection sensitivity of approximately 2.5 μg/mm², sufficient for detecting localized lithium accumulation.
  • Successfully extended μXRS from bulk-average measurements to spatially resolved quantification.

Conclusions:

  • The novel μXRS imaging system provides a powerful non-destructive tool for spatially resolved quantification of metallic lithium.
  • This advancement is critical for understanding Li-ion battery degradation mechanisms and enhancing operational safety.
  • The system offers a promising solution for battery safety inspection and other light-element imaging challenges.