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Microstructure Characteristics and Tribological Performances of LPBF-Processed TiCp/TA15 Composite.
Junwen Cao1,2, Yumeng Zhao1,2, Wentao Liu1,2,3
1China National Nuclear Corporation (CNNC) Key Laboratory on Fabrication Technology of Reactor Irradiation Special Fuel Assembly, Baotou 014035, China.
Heat treatment of titanium matrix composites (TMCs) significantly improves wear resistance. The enhanced microstructure reduces friction and wear rates by strengthening the material and preventing plastic deformation.
Area of Science:
- Materials Science
- Tribology
- Additive Manufacturing
Background:
- Microstructure and precipitate features are crucial for titanium matrix composites (TMCs) tribological performance.
- Laser powder bed fusion (LPBF) is an additive manufacturing technique used for fabricating TMCs.
Purpose of the Study:
- To investigate the influence of microstructural evolution on the tribological performance of TiCp/TA15 composites fabricated via LPBF.
- To understand the wear mechanisms of as-built and heat-treated TMCs.
Main Methods:
- Fabrication of TiCp/TA15 composites using LPBF.
- Heat treatment of the as-built composite at 750 °C for 2 h (HT-750) to achieve a uniform duplex (α + β) microstructure with enhanced TiC precipitation.
- Systematic investigation of microstructural evolution and tribological performance, including microhardness, friction coefficient, and wear rate.
Main Results:
- The HT-750 composite showed increased microhardness (459.2 ± 3.1 HV) compared to the as-built composite (360.2 ± 6.4 HV).
- The friction coefficient decreased from 0.649 ± 0.167 (as-built) to 0.581 ± 0.111 (HT-750).
- The wear rate significantly reduced from 8.24 ± 0.44 × 10⁻⁴ mm³/N·m (as-built) to 4.81 ± 0.39 × 10⁻⁴ mm³/N·m (HT-750), indicating enhanced wear resistance.
- The improved performance is attributed to the synergistic effect of the duplex matrix and TiC particles, enhancing load-bearing capacity and suppressing plastic deformation.
- Wear mechanisms differed: as-built composites experienced delamination, oxidative, and abrasive wear due to plastic deformation, while HT-750 composites showed dominant oxidative wear with minor abrasive wear and delamination.
Conclusions:
- Heat treatment at 750 °C significantly enhances the tribological performance of additively manufactured TiCp/TA15 composites.
- The duplex microstructure and TiC precipitation in HT-750 composites improve hardness and wear resistance by mitigating plastic deformation and damage.
- Understanding these microstructural-tribological relationships is key for designing advanced TMCs for demanding applications.
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