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Published on: February 3, 2018
JCp-1-NP: New and compiled LA-ICP-MS elemental compositional data of the nano-powdered reference material
Sebastian Flöter1, Frank Förster2, James Vincent3
1Department of Earth Sciences, University of Geneva, Genève, Switzerland. sebastian.floeter@unige.ch.
This study quantifies the elemental composition of JCp-1-NP, a calcium carbonate reference material crucial for Laser Ablation-Inductively Coupled Plasma-Mass Spectrometry (LA-ICP-MS). Findings provide essential data for accurate material characterization and analytical method validation.
Area of Science:
- Geochemistry
- Analytical Chemistry
- Materials Science
Background:
- JCp-1-NP is a pressed nano-powder pellet calcium carbonate reference material.
- It is widely used in Laser Ablation-Inductively Coupled Plasma-Mass Spectrometry (LA-ICP-MS).
- Its precise elemental composition and stability are not well-documented.
Purpose of the Study:
- To determine the uncertainty of the elemental composition of JCp-1-NP.
- To assess the long-term stability of this reference material.
- To compile and review all publicly available compositional data for JCp-1-NP.
Main Methods:
- Analysis of 20 element-to-calcium ratios.
- Interlaboratory comparison across three independent laboratories.
- Outlier correction of the dataset for robust assessment.
Main Results:
- A robust assessment of JCp-1-NP's composition and long-term stability was achieved.
- Uncertainty of key element-to-calcium ratios was quantified.
- A comprehensive review of existing compositional data was compiled.
Conclusions:
- The study provides critical, validated compositional data for the JCp-1-NP reference material.
- This enhances its reliability for LA-ICP-MS applications.
- The findings support accurate geochemical and materials science analyses.
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