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Updated: Aug 19, 2026

Magnetometric Characterization of Intermediates in the Solid-State Electrochemistry of Redox-Active Metal-Organic Frameworks
Published on: June 9, 2023
Synthesis of spinel@MOF self-supported nanoarray electrodes for electrochemical detection of H2O2
Jiawei Dai1, Yuchen Huang2, Deyu Zhu1
1School of Chemistry and Chemical Engineering, Hubei Key Laboratory of Material Chemistry and Service Failure, Key Laboratory of Material Chemistry for Energy Conversion and Storage (Ministry of Education), Huazhong University of Science and Technology (HUST), 1037 Luoyu Rd, Wuhan, 430074, China. guangfl@hust.edu.cn.
Abstract:
A self-supported CuCo2O4 spinel@CuCoHHTP-4/copper foam (CF) nanoarray electrode was synthesized successfully via partial mild pyrolysis of the well-known CuCoHHTP MOFs. CuCo2O4 spinel@CuCoHHTP-4/CF exhibits excellent electrochemical activity and stability towards H2O2, which is attributed to the strong Fenton-like reactivity of CuCo2O4 and the residual porosity of the MOF structure.
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