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High-performance liquid chromatographic assay of 8-hydroxyquinoline sulfate and its stability in immunobiological
A Mihajlović1, D Agbaba, D Zivanov-Stakić
1Control Department, TORLAK, Belgrade, Yugoslavia.
Journal of Chromatography. A
|May 2, 1998
Abstract:
Because of the ability of 8-hydroxyquinoline sulfate (8-HQS) to irreversibly bind metals from rubber stoppers, the stability of 8-HQS in tuberculin solutions was investigated. For the determination of 8-HQS, a simple and sensitive reversed-phase HPLC method with detection at 240 nm was developed and validated. Rapid decreases in concentrations of 8-HQS were found in samples stored in original vials which were exposed to different temperatures and vial positions.