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AAPS Pharmscitech|June 27, 2006
Heat and mass transfer scale-up issues during freeze-drying, III: control and characterization of dryer differences via operational qualification testsS Rambhatla, S Tchessalov, Michael J PikalJournal of Pharmaceutical Sciences|September 14, 2007
Use of manometric temperature measurement (MTM) and SMART freeze dryer technology for development of an optimized freeze-drying cycleHenning Gieseler, Tony Kramer, Michael J PikalJournal of Pharmaceutical Sciences|February 18, 2011
High-precision absolute (true) density measurements on hygroscopic powders by gas pycnometry: application to determining effects of formulation and process on free volume of lyophilized productsTakayuki Kikuchi, Bingquan Stuart Wang, Michael J PikalJournal of Pharmaceutical Sciences|February 2, 2008
Solid state 13C NMR investigation of impact of annealing in lyophilized glassesSuman A Luthra, Michael J Pikal, Marcel UtzJournal of Pharmaceutical Sciences|September 11, 2007
Effect of hydration on the secondary structure of lyophilized proteins as measured by fourier transform infrared (FTIR) spectroscopySumit Luthra, Devendra S Kalonia, Michael J PikalAAPS Pharmscitech|January 9, 2010
Determination of end point of primary drying in freeze-drying process controlSajal M Patel, Takayuki Doen, Michael J PikalJournal of Pharmaceutical Sciences|August 16, 2008
Solid state chemistry of proteins IV. What is the meaning of thermal denaturation in freeze dried proteins?Michael J Pikal, Daniel Rigsbee, Michael J AkersAAPS Pharmscitech|November 26, 2009
Reduced pressure ice fog technique for controlled ice nucleation during freeze-dryingSajal M Patel, Chandan Bhugra, Michael J PikalJournal of Pharmaceutical Sciences|August 26, 2010
The effect of dryer load on freeze drying process designSajal M Patel, Feroz Jameel, Michael J PikalJournal of Pharmaceutical Sciences|January 3, 2013
Investigations on polyplex stability during the freezing step of lyophilization using controlled ice nucleation--the importance of residence time in the low-viscosity fluid stateJulia C Kasper, Michael J Pikal, Wolfgang FriessPageof 17