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Updated: Jul 1, 2026

Methods to Identify the NMR Resonances of the 13C-Dimethyl N-terminal Amine on Reductively Methylated Proteins
13:59

Methods to Identify the NMR Resonances of the 13C-Dimethyl N-terminal Amine on Reductively Methylated Proteins

Published on: December 12, 2013

13C核オーバーハウザーの極化-マジック・アングル回転型核磁気共振スペクトロスコーピーは,均一に13Cでラベルを貼った固体タンパク質で実施されます

Etsuko Katoh1, K Takegoshi, Takehiko Terao

  • 1Biochemistry Department, National Institute of Agrobiological Sciences, Tsukuba, Ibaraki 305-8602, Japan.

Journal of the American Chemical Society
|March 18, 2004
PubMed
まとめ

NOP-MAS (Nuclear Overhauser Polarization-Magic Angle Spinning) は,クロス・ポラライゼーション (CP) よりも効果的にタンパク質内の (13) C信号を強化する. このテクニックは,定量分析を可能にし,移動分子や添加物を含むサンプルでうまく機能します.

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