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Updated: Jul 13, 2026

Methods to Identify the NMR Resonances of the 13C-Dimethyl N-terminal Amine on Reductively Methylated Proteins
13:59

Methods to Identify the NMR Resonances of the 13C-Dimethyl N-terminal Amine on Reductively Methylated Proteins

Published on: December 12, 2013

DEPTの極化移転における1J (CH) の依存をキャンセルすることによって,感度強化された定量的13C NMRスペクトロスコーピー

Terry J Henderson1

  • 1U.S. Army Edgewood Chemical Biological Forensic Analytical Center, AMSRD-ECB-RT-AF, E5100, 5183 Black Hawk Road, Aberdeen Proving Ground, Maryland 21010-5424, USA. txhender@apgea.army.mil

Journal of the American Chemical Society
|March 25, 2004
PubMed
まとめ

新しい核磁共鳴 (NMR) 方法は,炭素13 (13C) のスペクトルの信号強度の変動を排除し,定量分析を改善します. このテクニックは,13C NMR実験の感度を高め,取得時間を短縮します.

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¹H NMR of Labile Protons: Deuterium (²H) Substitution

This lesson illustrates the role of deuterium substitution in simplifying the NMR spectrum of compounds comprising labile protons. One method employed is the use of deuterium. Amongst the three isotopes of hydrogen, deuterium (2H) has a nucleus composed of one proton and one neutron. When the D2O solvent is added to a pure dry ethanol solution, its labile proton is substituted with deuterium.
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Carbon-13 (¹³C) NMR: Overview

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¹H NMR of Conformationally Flexible Molecules: Variable-Temperature NMR

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¹³C NMR: ¹H–¹³C Decoupling

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