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Updated: Jul 11, 2026

Structure and Coordination Determination of Peptide-metal Complexes Using 1D and 2D 1H NMR
14:44

Structure and Coordination Determination of Peptide-metal Complexes Using 1D and 2D 1H NMR

Published on: December 16, 2013

シンメトリーベースの29Si二極再結合マジック・アングル・スピニングNMRスペクトロスコピー:ゼオライト・フレームワークの3次元構造を調査するための新しい方法

Darren H Brouwer1, Per Eugen Kristiansen, Colin A Fyfe

  • 1School of Chemistry, University of Southampton, Southampton, United Kingdom, SO17 1BJ.

Journal of the American Chemical Society
|January 13, 2005
PubMed
まとめ

新しい29Si固体磁気共振 (MAS NMR) 実験は,純粋なシリカゼオライトのフレームワークの研究を強化します. この高度なNMR技術は,シリコン-酸素-シリコン結合と長距離のシリコン-シリコン距離を正確に決定し,未知のゼオライト構造を解明するのに役立ちます.

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¹H NMR: Complex Splitting01:13

¹H NMR: Complex Splitting

A proton M that is coupled to a proton X results in doublet signals for M. However, NMR-active nuclei can be simultaneously coupled to more than one nonequivalent nucleus. When M is coupled to a second proton A, such as in styrene oxide, each peak in the doublet is split into another doublet.
Splitting diagrams or splitting tree diagrams are routinely used to depict such complex couplings. While drawing splitting diagrams, the splitting with the larger coupling constant is usually applied first.
¹H NMR of Conformationally Flexible Molecules: Temporal Resolution00:52

¹H NMR of Conformationally Flexible Molecules: Temporal Resolution

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¹³C NMR: Distortionless Enhancement by Polarization Transfer (DEPT)

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Two-Dimensional (2D) NMR: Overview

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NMR Spectroscopy: Spin–Spin Coupling

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2D NMR: Overview of Homonuclear Correlation Techniques

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