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Updated: Jul 13, 2026

Split-and-pool Synthesis and Characterization of Peptide Tertiary Amide Library
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Published on: June 20, 2014

发现了使用分离连接的PTP1B的新型色胺模仿物

Daniel A Erlanson1, Robert S McDowell, Molly M He

  • 1Sunesis Pharmaceuticals, Inc., 341 Oyster Point Boulevard, South San Francisco, California 94080, USA. erlanson@sunesis.com

Journal of the American Chemical Society
|May 8, 2003
PubMed
概括

研究人员开发了"分离连接",以寻找蛋白质氨酸酸酶的新药抑制剂. 这种方法成功地发现了抗糖尿病蛋白PTP1B的新型铁模仿物.

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When proton-coupled carbon-13 spectra are simplified by a broadband proton decoupling technique, structural information about the coupled protons is lost. Distortionless enhancement by polarization transfer (DEPT) is a technique that provides information on the number of hydrogens attached to each carbon in a molecule. While the DEPT experiment utilizes complex pulse sequences, the pulse delay and flip angle are specifically manipulated. The resulting signals have different phases depending on...