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Metal-silicate Partitioning at High Pressure and Temperature: Experimental Methods and a Protocol to Suppress Highly Siderophile Element Inclusions
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Published on: June 13, 2015

冠石类型IN2O3环境压力合成

Mauro Epifani1, Pietro Siciliano, Alexander Gurlo

  • 1Istituto per la Microelettronica e i Microsistemi, IMM-CNR, Sezione di Lecce, Via Arnesano, 73100 Lecce, Italy.

Journal of the American Chemical Society
|April 1, 2004
PubMed
概括
此摘要是机器生成的。

研究人员在环境压力下合成了高压六边形 (III) 氧化物 (In2O3). 这种新的合成方法涉及沉和化,为氧化材料的应用提供了新的可能性.

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科学领域:

  • 材料科学 材料科学 材料科学
  • 无机化学 无机化学 有机化学
  • 固态化学 固态化学

背景情况:

  • (III) 氧化物 (In2O3) 通常存在于立方体或四角形相.
  • 冠状体类型 (六角形) In2O3 是一种高压多态.
  • 在环境条件下合成高压相具有科学意义.

研究的目的:

  • 在环境压力下报告高压冠状体类型In2O3相的形成.
  • 描述一种新的合成方法,用于生产六边形In2O3.3.
  • 调查影响这一阶段稳定性的因素.

主要方法:

  • 使用缩氨溶液在甲醇中沉酸.
  • 由此产生的沉物在250至500摄氏度的温度下化.
  • 对类型In2O3.3的形成和稳定机制的分析.

主要成果:

  • 在环境压力下成功合成了金刚石类型 (六角形) In2O3.
  • 合成是通过一种特殊的沉和化过程实现的.
  • 该研究讨论了杂质和添加剂在稳定六角In2O3相中的关键作用.

结论:

  • 在环境条件下可以形成高压六角In2O3.
  • 描述的方法为合成这种转移稳定阶段提供了一个可行的途径.
  • 了解杂质和添加剂的影响对于控制In2O3多态的形成至关重要.