Jove
Visualize
联系我们

相关概念视频

Atomic Mass01:52

Atomic Mass

Atoms — and the protons, neutrons, and electrons that compose them — are extremely small. For example, a carbon atom weighs less than 2 × 10−23 g. When describing the properties of tiny objects such as atoms, we use appropriately small units of measure, such as the atomic mass unit (amu). The amu was originally defined based on hydrogen, the lightest element, then later in terms of oxygen. Since 1961, it has been defined with regard to the most abundant isotope of carbon, atoms of which are...
Formula Mass and Mole Concepts of Compounds02:56

Formula Mass and Mole Concepts of Compounds

Formula Mass of Covalent Compounds
¹H NMR: Complex Splitting01:13

¹H NMR: Complex Splitting

A proton M that is coupled to a proton X results in doublet signals for M. However, NMR-active nuclei can be simultaneously coupled to more than one nonequivalent nucleus. When M is coupled to a second proton A, such as in styrene oxide, each peak in the doublet is split into another doublet.
Splitting diagrams or splitting tree diagrams are routinely used to depict such complex couplings. While drawing splitting diagrams, the splitting with the larger coupling constant is usually applied first.
Properties of Organometallic Compounds01:23

Properties of Organometallic Compounds

Organometallic compounds are compounds that contain a carbon–metal bond. Carbon belongs to an organyl group like alkyl, aryl, allyl, or benzyl groups. The metal can be from Group I or Group II of the periodic table, a transition metal, or a semimetal.
Characteristics and Nomenclature of Copolymers01:24

Characteristics and Nomenclature of Copolymers

Copolymers are the products obtained from the polymerization of multiple monomer species. So, in a polymer chain itself, there can be multiple repeating units that come from different monomers. The process of synthesizing a polymer from different monomer species is called copolymerization. When two monomers are involved, the polymer is known as a bipolymer. Polymers with three and four monomers are termed terpolymers and quaterpolymers, respectively. Figure 1 depicts the copolymerization of...
Mass Spectrum: Interpretation01:24

Mass Spectrum: Interpretation

An unknown compound can be established by identifying the molecular ion peak in the mass spectrum. The molecular ion peak is often weak or absent due to the predominance of fragmentation in high-energy electron beams. In such cases, a soft-energy electron beam can be used to scan the spectrum to enhance the intensity of the molecular ion peak. Additionally, chemical ionization, field ionization, and desorption ionization spectra are used to obtain a relatively intense molecular ion peak.To...

您也可能阅读

相关文章

通过共同作者、期刊和引用图与本文相关的文章。

排序
Same author

Comparison of Binary Alcohol/Water Solvent Systems to Blood for Extractions of Blood-Contacting Medical Devices.

PDA journal of pharmaceutical science and technology·2024
Same author

Super Stretchable and Compressible Hydrogels Inspired by Hook-and-Loop Fasteners.

Langmuir : the ACS journal of surfaces and colloids·2021
Same author

Reducing relative response factor variation using a multidetector approach for extractables and leachables (E&L) analysis to mitigate the need for uncertainty factors.

Journal of pharmaceutical and biomedical analysis·2020
Same author

Qualitative assessment of extractables from single-use components and the impact of reference standard selection.

Journal of pharmaceutical and biomedical analysis·2017
Same author

Gold nanoparticles with externally controlled, reversible shifts of local surface plasmon resonance bands.

Langmuir : the ACS journal of surfaces and colloids·2009
Same author

Poly(allylamine)-encapsulated water-soluble CdSe nanocrystals.

The journal of physical chemistry. B·2007
JoVE
x logofacebook logolinkedin logoyoutube logo
关于 JoVE
概览领导团队博客JoVE 帮助中心
作者
出版流程编辑委员会范围与政策同行评审常见问题投稿
图书馆员
用户评价订阅访问资源图书馆顾问委员会常见问题
研究
JoVE JournalMethods CollectionsJoVE Encyclopedia of Experiments存档
教育
JoVE CoreJoVE BusinessJoVE Science EducationJoVE Lab Manual教师资源中心教师网站
使用条款与条件
隐私政策
政策

相关实验视频

Updated: Jul 12, 2026

A Simple and Efficient Protocol for the Catalytic Insertion Polymerization of Functional Norbornenes
09:08

A Simple and Efficient Protocol for the Catalytic Insertion Polymerization of Functional Norbornenes

Published on: February 27, 2017

量化确定二氧化-多聚 ((norbornene) 纳米复合材料的化学成分.

Mark Anderson Jordi1, Thomas A P Seery

  • 1Department of Chemistry and Polymer Program, University of Connecticut, Storrs, Connecticut 06269, USA.

Journal of the American Chemical Society
|March 24, 2005
PubMed
概括

研究人员使用环开放型转化聚合 (ROMP) 制造了纳米粒子混合材料. 他们精确量化了复合材料的形成,使得可以控制高分子刷密度,用于先进的材料应用.

科学领域:

  • 材料科学 材料科学 材料科学
  • 聚合物化学 聚合物化学
  • 纳米技术纳米技术

背景情况:

  • 纳米粒子混合材料通过将无机芯与有机聚合物外相结合,提供独特的特性.
  • 控制纳米粒子表面的聚合物刷密度对于定制材料性能至关重要.
  • 环开元化聚合 (ROMP) 是一种用于聚合物合成的多功能技术.

研究的目的:

  • 使用ROMP制备二氧化核心/多聚 (norbornene) 刷纳米粒子混合材料.
  • 量化确定每个复合材料形成阶段的效率.
  • 为了证明对纳米粒子表面的聚合物链密度的控制.

主要方法:

  • 合成用于ROMP的功能化芯纳米粒子.
  • 对表面结合的功能组,催化剂负荷和聚合物链密度的定量分析.
  • 控制反应时间和表面功能群密度的变化,以调整链密度.

主要成果:

  • 通过ROMP成功制备了芯/聚 (norbornene) 刷混合纳米颗粒.
  • 对反应效率和启动分量的定量评估.
  • 通过反应时间和表面功能化来证明对聚合物刷密度的控制.
  • 实现了广泛的刷密度,与其他聚合物接种方法相美.

更多相关视频

Photogeneration of N-Heterocyclic Carbenes: Application in Photoinduced Ring-Opening Metathesis Polymerization
12:19

Photogeneration of N-Heterocyclic Carbenes: Application in Photoinduced Ring-Opening Metathesis Polymerization

Published on: November 29, 2018

Controlling Particle Fraction in Microporous Annealed Particle Scaffolds for 3D Cell Culture
08:11

Controlling Particle Fraction in Microporous Annealed Particle Scaffolds for 3D Cell Culture

Published on: October 28, 2022

相关实验视频

Last Updated: Jul 12, 2026

A Simple and Efficient Protocol for the Catalytic Insertion Polymerization of Functional Norbornenes
09:08

A Simple and Efficient Protocol for the Catalytic Insertion Polymerization of Functional Norbornenes

Published on: February 27, 2017

Photogeneration of N-Heterocyclic Carbenes: Application in Photoinduced Ring-Opening Metathesis Polymerization
12:19

Photogeneration of N-Heterocyclic Carbenes: Application in Photoinduced Ring-Opening Metathesis Polymerization

Published on: November 29, 2018

Controlling Particle Fraction in Microporous Annealed Particle Scaffolds for 3D Cell Culture
08:11

Controlling Particle Fraction in Microporous Annealed Particle Scaffolds for 3D Cell Culture

Published on: October 28, 2022

结论:

  • ROMP提供了一种强大的方法,用于创建定义良好的纳米粒子混合材料.
  • 定量分析可以精确控制聚合物刷架构.
  • 开发的方法为纳米技术和材料科学中的各种应用提供可调节的聚合物密度.