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Updated: Jun 8, 2026

Synthesis of a Thiol Building Block for the Crystallization of a Semiconducting Gyroidal Metal-sulfur Framework
12:30

Synthesis of a Thiol Building Block for the Crystallization of a Semiconducting Gyroidal Metal-sulfur Framework

Published on: April 9, 2018

通过超声波辅助的合成,直接从液体中获得大型,高质量的硫酸单晶

Boaz Pokroy1, Barbara Aichmayer, Anna Sophia Schenk

  • 1Department of Materials Engineering and Russell Berrie Nanotechnology Institute, Technion Israel Institute of Technology, Haifa 32000, Israel. bpokroy@tx.technion.ac.il

Journal of the American Chemical Society
|September 30, 2010
PubMed
概括

研究人员开发了一种快速的方法,通过超声波从液体中直接合成大型硫酸晶体. 这种新技术提供了一种更快,更有效的方法来生产高质量的硫酸盐晶体,用于结构分析.

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Compact Quantum Dots for Single-molecule Imaging17:14

Compact Quantum Dots for Single-molecule Imaging

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The Synthesis of [Sn10(Si(SiMe3)3)4]2- Using a Metastable Sn(I) Halide Solution Synthesized via a Co-condensation Technique12:43

The Synthesis of [Sn10(Si(SiMe3)3)4]2- Using a Metastable Sn(I) Halide Solution Synthesized via a Co-condensation Technique

Published on: November 28, 2016

相关概念视频

Preparation and Reactions of Thiols02:33

Preparation and Reactions of Thiols

Thiols are prepared using the hydrosulfide anion as a nucleophile in a nucleophilic substitution reaction with alkyl halides. For instance, bromobutane reacts with sodium hydrosulfide to give butanethiol.
Preparation and Reactions of Sulfides02:26

Preparation and Reactions of Sulfides

Sulfides are the sulfur analog of ethers, just as thiols are the sulfur analog of alcohol. Like ethers, sulfides also consist of two hydrocarbon groups bonded to the central sulfur atom. Depending upon the type of groups present, sulfides can be symmetrical or asymmetrical. Symmetrical sulfides can be prepared via an SN2 reaction between 2 equivalents of an alkyl halide and one equivalent of sodium sulfide.