使用太赫兹光谱学测定热水处理后大米粉晶度的变化
Han Guo1, Keiichiro Shiraga2, Naoshi Kondo1
1Graduate School of Agriculture, Kyoto University, Kitashirakawa-Oiwakecho, Sakyo-ku, Kyoto 606-8502, Japan.
Food chemistry
|May 27, 2023
概括
富里埃变换特拉赫兹 (FT-THz) 谱学可以量化热湿处理 (HMT) 后的米粉结晶度的变化. 特定的太赫兹峰值与A型和Vh型晶体结构相关,使得精确的分析成为可能.
科学领域:
- 食品科学与技术 食品科学与技术
- 材料科学是一种材料科学.
- 频谱学是一种光谱学.
背景情况:
- 在热水处理 (HMT) 过程中,粉经历结构变化.
- 米粉中的结晶性包括A型和Vh型结构,特别是在粉脂复合体 (ALC) 中.
- 了解这些结构转变对于食品加工和材料表征至关重要.
研究的目的:
- 评估富里埃变换太赫兹 (FT-THz) 光谱在监测HMT后的米粉晶度变化的有效性.
- 建立THz光谱特征和特定晶体结构 (A型和Vh型) 之间的相关性.
主要方法:
- 米粉样本经过热水处理 (HMT).
- 使用X射线衍射 (XRD) 谱法评估了结晶性.
- 收购和分析了太赫兹 (THz) 频谱,重点是衍生频谱.
主要成果:
- 在9.0 THz的第二个衍生THz峰值的强度和A型和Vh型晶度之间观察到强烈的相关性.
- 额外的THz峰值为10.5 THz,12.2 THz和13.1 THz,表明对Vh型晶体结构的敏感性.
结论:
- FT-THz光谱是一种可行的方法,用于量化HMT后大米粉中的A型粉和ALC (Vh型) 晶度.
- 特定的THz光谱特征可以作为处理过的米粉中不同晶体形式的可靠标记.
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