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周边程序以产生平均相当面积的粒度大小
Wei-Jie Qiu1, Xuan-Wei Lei2, Yu Zhang1
1Faculty of Materials, Metallurgy and Chemistry, Jiangxi University of Science and Technology, Ganzhou 341000, China.
Ultramicroscopy
|June 28, 2023
概括
一个新的周边程序准确地从定向成像显微镜 (OIM) 数据中确定平均颗粒大小. 这种方法即使与颗粒大小相对较大的像素大小也能提供可靠的结果,从而增强了材料分析.
科学领域:
- 材料科学 材料科学 材料科学
- 金属学金属学是什么
- 显微镜的使用方法
背景情况:
- 精确的颗粒大小测量对于了解材料特性至关重要.
- 现有的方法可能会在不同的像素大小和粒度形态方面扎.
- 定向成像显微镜 (OIM) 提供了详细的微观结构信息.
研究的目的:
- 开发和验证一个新的周边程序,用于计算平均相当面积的粒度大小.
- 在不同的实验条件下评估周边程序的可靠性.
- 为了比较周边程序与已建立的方法,如拦截,平面测量和统计方法.
主要方法:
- 开发了一个新的周边程序公式:r ̄p=(2AmPm+wb2Es) ±wb2Es.
- 使用商业软件测量谷物面积 (Am) 和周边 (Pm).
- 进行了各种各样的粒形,EBSD步骤大小和粒边界宽度的实验.
主要成果:
- 周边程序产生了平均颗粒大小测量,在所有测试条件下保持一致并接近真实值.
- 结果证明了周边程序的稳定性.
- 该方法证明有效,即使EBSD步骤大小 (Es) 与粒径相比相对较大.
结论:
- 开发的周边程序提供了一种可靠的方法,用于从OIM数据中确定平均相当面积的粒度大小.
- 这种技术具有稳定性和准确性的优势,特别是在具有较大的像素与粒度比率的场景中.
- 周边程序提高了材料科学中的微结构分析的精度.
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