用LC-ICP-MS确定食用昆虫中的物种
Eri Matsumoto1, Makoto Matsumoto1
1Japan Food Research Laboratories, 6-11-10 Nagayama, Tama-shi, Tokyo 206-0025, Japan.
Journal of AOAC International
|July 14, 2023
概括
可食用昆虫可能含有,含量因物种而异. 控制昆虫的料至关重要,因为含量通常取决于它们的饮食.
科学领域:
- 食品科学 食品科学 食品科学
- 分析化学 分析化学
- 环境科学 环境科学
背景情况:
- 可食用昆虫是食的潜在来源.
- 准确评估暴露需要对特定物种进行分析.
研究的目的:
- 验证一种分析方法,用于确定和量化食用昆虫中的物种.
- 评估各种可食用昆虫物种的含量和物种化.
主要方法:
- 使用0.3mol/L酸和在100°C加热的物种的提取.
- 通过液体染色学-诱导合等离子体质谱法 (LC-ICP-MS) 进行量化.
- 在移动阶段使用了带有离子对试剂的八甲基西兰 (ODS) 柱.
主要成果:
- 经过验证的LC-ICP-MS方法证明了令人满意的检测 (LOD) 和量化 (LOQ) 极限,可重复性,中间精度和准确性.
- 无机是大多数可食用昆虫样本中检测到的占主导地位的物种.
- 的度在物种之间差异很大,甲虫的度特别高.
结论:
- 可食用昆虫中的含量取决于物种,并受到它们的饮食的影响.
- 有效的料管理对于控制食用昆虫产品中的含量至关重要.
更多相关视频
08:56Detection of Regulated Ergot Alkaloids in Food Matrices by Liquid Chromatography-Trapped Ion Mobility Spectrometry-Time-of-Flight Mass Spectrometry
Published on: November 22, 2024
688
08:01Removal of Arsenic Using a Cationic Polymer Gel Impregnated with Iron Hydroxide
Published on: June 28, 2019
7.6K
相关概念视频
Inductively Coupled Plasma-Mass Spectrometry (ICP-MS): Interferences
524
Inductively coupled plasma–mass spectrometry (ICP–MS) is a highly selective and sensitive technique for accurate elemental analysis. Though the analysis of ICP–MS mass spectra is comparatively straightforward, it is affected by spectroscopic and non-spectroscopic interferences. Spectroscopic interferences arise when the plasma contains ionic species with an m/z value the same as the analyte ion. Spectroscopic interference can be categorized as isobaric, polyatomic ions, and...
524
Atomic Absorption Spectroscopy: Lab
495
For AAS measurements, samples must be introduced as clear solutions, often requiring extensive preliminary treatment to dissolve materials like soils, animal tissues, and minerals. Common methods for sample preparation include treatment with hot mineral acids, wet ashing, combustion in closed containers, high-temperature ashing, or fusion with reagents.
Solutions containing organic solvents, such as low-molecular-mass alcohols, esters, or ketones, enhance absorbances by increasing...
Solutions containing organic solvents, such as low-molecular-mass alcohols, esters, or ketones, enhance absorbances by increasing...
495
