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使用GC-FID应用相对摩尔敏感度方法来量化沙夫兰 (Crocus sativus L.) 中的沙夫兰

Naoko Masumoto¹, Takumi Ohno², Toshihiro Suzuki²

¹Division of Food Additives, National Institute of Health Sciences, 3-25-26, Tonomachi, Kawasaki-Ku, Kawasaki, Kanagawa, 210-9501, Japan. nasato@nihs.go.jp.

Journal of natural medicines

|July 14, 2023

概括

准确量化沙夫兰的数量.

科学领域:

分析化学分析化学
食品化学食品化学
自然产品分析自然产品分析

背景情况:

沙夫兰是沙夫兰质量的关键化合物,但其挥发性和降解使准确的量化复杂化.
对于已知纯度的萨夫兰的商业分析标准是不可用的,这阻碍了精确的测量.

研究的目的:

开发和验证一种用于准确量化沙夫兰中沙夫兰的新方法.
建立一种可靠的分析方法,克服现有方法的局限性.

主要方法:

开发了一种使用GC-FID的相对摩尔敏感度 (RMS) 方法.
使用定量NMR和染色学确定沙夫拉纳相对于认证的参考材料 (1,4-bis(trimethylsilyl) benzene-d4) 的RMS.
在不同的GC-FID仪器中验证了该方法,以评估仪器间的影响.

主要成果:

该RMS方法实现了高精度 (99.4-101%) 和出色的重复性 (0.81%).
工具间的差异是微小的 (0.6%),表明了稳健性.
GC-FID化气被确定为影响RMS和定量结果的因素.

结论:

与传统的校准曲线和光谱法相比,RMS方法提供了一个更准确和可靠的方法来定量沙夫兰.
这种方法解决了沙夫兰的不稳定性和缺乏纯标准所带来的挑战.
了解GC-FID参数的影响,如化气,对于精确的沙夫兰分析至关重要.

关键词:

1H-定量性NMR的使用方法.克罗库斯 (Crocus sativus) 是一种植物.在 GC-FID 中.相对摩拉敏感度相对摩拉敏感度撒法伦是什么意思撒法伦是什么意思萨夫拉纳尔是一种安全的药物.

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