通过软溶液加工持续生产功能化石墨烯墨水
Kodepelly Sanjeeva Rao1, Jaganathan Senthilnathan1,2, Jyh-Ming Ting1
1Promotion Center for Global Materials Research (PCGMR), Department of Material Science and Engineering, National Cheng Kung University, Tainan 701, Taiwan.
Nanomaterials (Basel, Switzerland)
|July 29, 2023
概括
我们开发了一种两阶段的方法,用于连续生产功能化石墨烯纳米板 (N-FG). 这个过程可以通过溶液加工直接生产N-FG油墨,简化了石墨烯的功能化.
科学领域:
- 材料科学 材料科学 材料科学
- 化学工程是化学工程的重要组成部分.
- 纳米技术 纳米技术
背景情况:
- 石墨烯纳米板 (GNSs) 需要有效的功能化,用于先进的应用.
- 现有的石墨烯功能化的方法往往涉及复杂的后处理步骤.
研究的目的:
- 开发一种基于溶液的连续方法,用于生产功能化石墨烯纳米板 (N-FG).
- 为了证明N-FG在没有干燥或削的情况下简化加工成油墨.
主要方法:
- 一个两阶段的反应:使用甘氨酸二硫酸离子复合物的电化学剥离石墨,以产生少数层的GNS,然后使用微波辅助功能化,使用azobisisobutyronitrile.
- 使用拉曼光谱和X射线光电子光谱 (XPS) 进行表征,以确认的结合.
主要成果:
- 通过Raman和XPS.成功合成了功能化石墨烯 (N-FG),通过Raman和XPS.确认了组插入.
- 在合成后,N-FG在各种溶剂 (DMF,乙烯基醇,乙烯,水) 中的可扩散性显著提高.
- 通过简单的洗-离心-分散序列展示直接的N-FG油墨生产,避免干燥和削.
结论:
- 该研究提出了一种新的"连续溶液加工"方法,用于N-FG油墨.
- 这种方法绕过了复杂的后处理,为石墨烯功能化和油墨配方提供了更绿色和更有效的途径.
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