激光覆盖的中等度FeNiCr-B4C涂层的机械和结构特征
Artem Okulov1, Yury Korobov1, Alexander Stepchenkov1
1M.N. Mikheev Institute of Metal Physics, Ural Branch of the Russian Academy of Sciences, 620108 Ekaterinburg, Russia.
Materials (Basel, Switzerland)
|August 12, 2023
概括
将碳化物 (B4C) 添加到等原子中型合金 (MEA) FeNiCr 涂层中,可显著提高微硬度. 这项研究表明B4C作为激光覆盖MEA涂层的有希望的增强剂.
科学领域:
- 材料科学 材料科学 材料科学
- 金工业是金工业的一个方面.
- 表面工程是什么?表面工程是什么?
背景情况:
- 中等合金 (MEAs) 为高级应用提供可调节的性能.
- 激光覆盖是沉积保护涂层的关键技术.
- 碳化物 (B4C) 以其硬度和强化金属矩阵的潜力而闻名.
研究的目的:
- 研究B4C添加剂对激光涂层FeNiCr MEA涂层的微观结构和机械性能的影响.
- 评估B4C作为这些涂料中强化剂的潜力.
- 描述FeNiCr矩阵内的B4C的相结构和结合.
主要方法:
- 使用脉冲激光覆盖,将FeNiCr-B4C涂层 (0,1,3重%B4C) 沉积在AISI 1040钢上.
- 扫描电子显微镜 (SEM) 分析了涂层的微观结构和厚度.
- 通过X射线衍射 (XRD) 和传输电子显微镜 (TEM) 确定了相组合和结构.
- 拉曼光谱证实了B4C的存在.
- 微硬度和柔性测试评估了机械性能.
主要成果:
- 涂层表现出均的厚度 (400 ± 20 μm) 与一个狭窄的基板过渡区.
- XRD证实了单面中心立方体 (FCC) γ-阶段,而TEM显示了3 wt.% B4C涂层中的两相FCC结构.
- 拉曼光谱通过特征性的C-B-C拉伸和无形碳峰值证实了B4C的存在.
- 微硬度增加了16% (1重量%B4C) 和38% (3重量%B4C).
- 柔性略微下降了4% (1重%B4C) 和10% (3重%B4C) 的情况.
结论:
- B4C添加是加强激光覆盖的FeNiCr MEA涂层的有效策略.
- 增强的微硬度伴随着柔性略有降低.
- 该研究强调了针对耐磨应用的定制MEA-B4C复合材料的潜力.
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