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来自X射线衍射的六边形La1-SrMnO3 (x = 0.3) 纳米颗粒的晶体大小的确定 - - 一项比较研究
Do Hung Manh1,2, Tran Thi Ngoc Nha2, Le Thi Hong Phong1
1Institute of Materials Science, Vietnam Academy of Science and Technology 18-Hoang Quoc Viet Hanoi City Vietnam thanhxraylab@yahoo.com.
RSC advances
|August 24, 2023
概括
在La0.7Sr0.3MnO3纳米颗粒中的晶石尺寸使用多种X射线衍射方法确定. 化温度影响纳米粒子结晶和弹性特性.
科学领域:
- 材料科学 材料科学 材料科学
- 纳米技术纳米技术
- 固态物理 固态物理
背景情况:
- 纳米材料的特性取决于晶体的尺寸和缺陷.
- 六角形La1-xSrxMnO3 (x=0.3) 是一种具有可调节的电子,磁,光学和弹性的材料.
研究的目的:
- 为了确定六边形La0.7Sr0.3MnO3纳米颗粒的晶体尺寸.
- 为了研究化温度对纳米粒子结晶的影响.
- 为了比较不同的X射线衍射方法来确定晶体的尺寸和弹性性质.
主要方法:
- 通过高能球磨法合成单相La0.7Sr0.3MnO3纳米粉.
- 在700°C和800°C时,纳米粉末的化.
- 采用X射线衍射 (XRD) 峰值扩展分析,使用修改的谢勒,威廉森-霍尔,大小-应变和哈尔德-瓦格纳方法.
主要成果:
- 结晶石的大小和弹性特性 (应变,应力,能量密度) 从XRD数据计算出来.
- 通过比较不同分析方法获得的结果,发现了差异.
- 观察到的结晶体大小差异归因于每个分析技术的不同方法.
结论:
- 多种基于XRD的方法提供了对La0.7Sr0.3MnO3纳米颗粒的晶体尺寸和弹性特性的洞察.
- 由于固有的技术差异,方法的选择会影响计算的晶石大小.
- 化温度在这些纳米粒子的结晶过程中起着重要作用.
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